n-Heptyl--d7 Alcohol

Base Information

• Chemical Name: n-Heptyl--d7 Alcohol
• CAS No.: 1219804-99-5
• Molecular Formula: CD3CD2CD2(CH2)4OH
• Molecular Weight: 123.25
• Mol file: 1219804-99-5.mol

Synonyms:

Chemical Property of n-Heptyl--d7 Alcohol

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

n-Heptyl-5,5,6,6,7,7,7-d7Alcohol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: n-Heptyl-5,5,6,6,7,7,7-d7 Alcohol (CAS# 1219804-99-5) is a useful isotopically labeled research compound.

Technology Process of n-Heptyl--d7 Alcohol

There total 6 articles about n-Heptyl--d7 Alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.8%

C7(2)H14O2 (158778-83-7,130348-93-5,352431-36-8) → heptanol-d16 (158778-86-0,1219804-99-5,194793-95-8)

Guidance literature:

With lithium aluminium deuteride; In diethyl ether; for 8h; Heating;

Reference yield:

<(2)H11>Pentyl bromide (126840-21-9,1219803-61-8,148404-92-6) → heptanol-d16 (158778-86-0,1219804-99-5,194793-95-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) EtONa / 1.) EtOH, 50 deg C, 1 h, 2.) EtOH, 30 deg C, 6 h

2: 1.) D₂O, NaOD, 2.) D₂SO₄ / 1.) reflux, 6 h, 2.) reflux, 4.5 h

3: 90.8 percent / LiAlD₄ / diethyl ether / 8 h / Heating

With lithium aluminium deuteride; deuteriated sodium hydroxide; water-d2; sodium ethanolate; sulfuric acid-d2; In diethyl ether;

Reference yield:

1-pentanol-d12 (158778-85-9,64118-19-0) → heptanol-d16 (158778-86-0,1219804-99-5,194793-95-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 83.7 percent / red phosphorous, Br₂ / 85 - 90 °C

2: 1.) EtONa / 1.) EtOH, 50 deg C, 1 h, 2.) EtOH, 30 deg C, 6 h

3: 1.) D₂O, NaOD, 2.) D₂SO₄ / 1.) reflux, 6 h, 2.) reflux, 4.5 h

4: 90.8 percent / LiAlD₄ / diethyl ether / 8 h / Heating

With phosphorus; lithium aluminium deuteride; deuteriated sodium hydroxide; bromine; water-d2; sodium ethanolate; sulfuric acid-d2; In diethyl ether;

upstream raw materials:

C₇⁽²⁾H₁₄O₂

<(2)H11>Pentyl bromide

1-pentanol-d12

pentanoic acid-d10

Downstream raw materials:

n-heptyl-d₁₅-bromide

Refernces