tert-Butyl 3-aminopropyl(isopropyl)carbamate

Base Information

• Chemical Name: tert-Butyl 3-aminopropyl(isopropyl)carbamate
• CAS No.: 1111236-12-4
• Molecular Formula: C₁₁H₂₄N₂O₂
• Molecular Weight: 216.324
• Hs Code.: 2924199090
• Mol file: 1111236-12-4.mol

Synonyms:tert-butyl 3-aminopropyl(isopropyl)carbamate;tert-butyl N-(3-aminopropyl)-N-(propan-2-yl)carbamate;Carbamic acid, N-(3-aminopropyl)-N-(1-methylethyl)-, 1,1-dimethylethyl ester

Chemical Property of tert-Butyl 3-aminopropyl(isopropyl)carbamate

Chemical Property:

• PSA: 55.56000
• LogP: 2.68100
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

tert-ButylN-(3-Aminopropyl)-N-(propan-2-yl)carbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-Butyl 3-aminopropyl(isopropyl)carbamate

There total 1 articles about tert-Butyl 3-aminopropyl(isopropyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.3%

C25H36N2O2 (1111236-11-3) → (3-amino-propyl)-isopropyl-carbamic acid tert-butyl ester (1111236-12-4)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃;

Reference yield: 91.0%

4-chloro-7H-pyrrolo[2,3-d]pyrimidine-5-carbaldehyde + formaldehyd (50-00-0,30525-89-4,61233-19-0) + (3-amino-propyl)-isopropyl-carbamic acid tert-butyl ester (1111236-12-4) → C17H26ClN5O2

Guidance literature:

4-chloro-7H-pyrrolo[2,3-d]pyrimidine-5-carboxaldehyde; (3-amino-propyl)-isopropyl-carbamic acid tert-butyl ester; With sodium tris(acetoxy)borohydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 16h;

formaldehyd; With water; sodium tris(acetoxy)borohydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 16h;

With water; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

(3-amino-propyl)-isopropyl-carbamic acid tert-butyl ester (1111236-12-4) + 4-[5-(2,3-dichloro-phenyl)-2-methyl-2H-pyrazol-3-yl]-piperidine-1-carbonyl chloride (550378-12-6) → [3-({4-[5-(2,3-dichloro-phenyl)-2-methyl-2H-pyrazol-3-yl]-piperidine-1-carbonyl}-amino)-propyl]-isopropyl-carbamic acid tert-butyl ester

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1016/j.bmcl.2004.12.045

upstream raw materials:

C₂₅H₃₆N₂O₂

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