1,2,4,5-Tetrahydrobenzo[d]oxepine

Base Information

• Chemical Name: 1,2,4,5-Tetrahydrobenzo[d]oxepine
• CAS No.: 5368-66-1
• Molecular Formula: C10H12O
• Molecular Weight: 148.205
• Hs Code.: 2932999099
• Mol file: 5368-66-1.mol

Synonyms:5-Oxabenzocyclohepten;1,2,4,5-Tetrahydrobenzo[d]oxepine;1,2,4,5-tetrahydro-3-benzoxepin;Tetrahydro-3-benzoxepin;5,6,8,9-tetrahydro-7-oxa-benzocycloheptene;

Chemical Property of 1,2,4,5-Tetrahydrobenzo[d]oxepine

Chemical Property:

• PSA: 9.23000
• LogP: 1.80180
• Storage Temp.: 2-8°C

Purity/Quality:

≥95% ^*data from raw suppliers

1,2,4,5-tetrahydrobenzo[d]oxepine 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2,4,5-Tetrahydrobenzo[d]oxepine

There total 7 articles about 1,2,4,5-Tetrahydrobenzo[d]oxepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-Methoxyethyl)benzaldehyde tosylhydrazone (119367-74-7) → isochromane (493-05-0) + 1,2,4,5-tetrahydrobenzo[d]oxepine (5368-66-1) + indan-2-yl methyl ether (81887-53-8) + 1-(2-Methoxyethyl)-2-(methoxymethyl)benzene (15018-15-2)

Guidance literature:

With sodium methylate; In methanol; for 2h; Yield given. Further byproducts given. Yields of byproduct given; Ambient temperature; Irradiation;

DOI:10.1021/ja00186a048

Reference yield:

C17H19N2O3S(1-)*Na(1+) (119391-26-3) → isochromane (493-05-0) + 1,2,4,5-tetrahydrobenzo[d]oxepine (5368-66-1) + indan-2-yl methyl ether (81887-53-8) + 7-(Methoxymethyl)bicyclo<4.2.0>octa-1,3,5-triene (119367-76-9)

Guidance literature:

at 320 ℃; under 0.001 Torr; Yield given. Further byproducts given. Yields of byproduct given;

DOI:10.1021/ja00186a048

Reference yield:

C17H19N2O3S(1-)*Na(1+) (119391-26-3) → isochromane (493-05-0) + 1,2,4,5-tetrahydrobenzo[d]oxepine (5368-66-1) + 7-(Methoxymethyl)bicyclo<4.2.0>octa-1,3,5-triene (119367-76-9) + 1-(Ethoxymethyl)-2-(2-methoxyethyl)benzene (119367-77-0)

Guidance literature:

In diethylene glycol dimethyl ether; for 2h; Yield given. Further byproducts given. Yields of byproduct given; Ambient temperature; Irradiation;

DOI:10.1021/ja00186a048

upstream raw materials:

2-(2-Methoxyethyl)benzaldehyde tosylhydrazone

C₁₇H₁₉N₂O₃S^(1-)*Na⁽¹⁺⁾

1,2-Phenylenediacetic acid

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