Dichloro[(S)-4,4'-bis[di(3,5-xylyl)phosphino]-2,2',6,6'-tetramethoxy-3,3'-bipyridine](p-cymene)ruthenium(II)

Base Information

• Chemical Name: Dichloro[(S)-4,4'-bis[di(3,5-xylyl)phosphino]-2,2',6,6'-tetramethoxy-3,3'-bipyridine](p-cymene)ruthenium(II)
• CAS No.: 1036379-70-0
• Molecular Formula: C₅₆H₆₄Cl₂N₂O₄P₂Ru
• Molecular Weight: 1063.06
• Mol file: 1036379-70-0.mol

Synonyms:

Chemical Property of Dichloro[(S)-4,4'-bis[di(3,5-xylyl)phosphino]-2,2',6,6'-tetramethoxy-3,3'-bipyridine](p-cymene)ruthenium(II)

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dichloro[(S)-4,4'-bis[di(3,5-xylyl)phosphino]-2,2',6,6'-tetramethoxy-3,3'-bipyridine](p-cymene)ruthenium(II)

There total 1 articles about Dichloro[(S)-4,4'-bis[di(3,5-xylyl)phosphino]-2,2',6,6'-tetramethoxy-3,3'-bipyridine](p-cymene)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 (52462-29-0) + (S)-2,2',6,6'-tetramethoxy-4,4'-bis(di(3,5-xylyl)phosphino)-3,3'-bipyridine (443347-10-2) → [RuCl(p-cymene)((R)-xylyl-P-phos)]Cl (1034001-49-4,1036379-70-0)

Guidance literature:

In methanol; at 50 ℃; for 2h; Inert atmosphere;

Reference yield:

[RuCl(p-cymene)((R)-xylyl-P-phos)]Cl (1034001-49-4,1036379-70-0) + (S)-1-isopropyl-2,2-bis(4-methoxyphenyl)ethylenediamine (148369-91-9) → RuCl[(S)-xylyl-p-phos][(S)-daipen]

Guidance literature:

With triethylamine; at 60 ℃; for 6h; Inert atmosphere;

upstream raw materials:

[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

(S)-2,2',6,6'-tetramethoxy-4,4'-bis(di(3,5-xylyl)phosphino)-3,3'-bipyridine

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