2,6-Bis(dodecyloxy)benzaldehyde

Base Information

• Chemical Name: 2,6-Bis(dodecyloxy)benzaldehyde
• CAS No.: 1198467-57-0
• Molecular Formula: C31H54O3
• Molecular Weight: 474.768
• Mol file: 1198467-57-0.mol

Synonyms:2,6-di(dodecyloxy)benzaldehyde;2,6-bis(dodecyloxy)benzaldehyde;2,6-di(dodecyloxy)benzealdehyde;

Chemical Property of 2,6-Bis(dodecyloxy)benzaldehyde

Chemical Property:

• PSA: 35.53000
• LogP: 10.09850
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2,6-Bis(dodecyloxy)benzaldehyde 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-Bis(dodecyloxy)benzaldehyde

There total 6 articles about 2,6-Bis(dodecyloxy)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1,3-bis(dodecyloxy)benzene (41662-92-4) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 2,6-di(dodecyloxy)benzealdehyde (1198467-57-0)

Guidance literature:

1,3-bis(dodecyloxy)benzene; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; at 0 - 20 ℃; Inert atmosphere;

N,N-dimethyl-formamide; In diethyl ether; hexane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/la9031927

Reference yield: 78.0%

1-Iodododecane (4292-19-7) + 1,3-bis(dodecyloxy)benzene (41662-92-4) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 2,6-di(dodecyloxy)benzealdehyde (1198467-57-0)

Guidance literature:

1-Iodododecane; 1,3-bis(dodecyloxy)benzene; With n-butyllithium;

N,N-dimethyl-formamide; In N,N-dimethyl-formamide;

With water;

DOI:10.1016/j.dyepig.2019.107597

Reference yield:

recorcinol (108-46-3) → 2,6-di(dodecyloxy)benzealdehyde (1198467-57-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / dimethyl sulfoxide / Inert atmosphere; Schlenk technique

2: n-butyllithium; N,N-dimethyl-formamide / diethyl ether / Inert atmosphere; Schlenk technique

With n-butyllithium; N,N-dimethyl-formamide; potassium hydroxide; In diethyl ether; dimethyl sulfoxide;

DOI:10.1142/S1088424614500308

upstream raw materials:

1,3-bis(dodecyloxy)benzene

N,N-dimethyl-formamide

recorcinol

1-dodecylbromide

Downstream raw materials:

meso-(2,6-di(dodecyloxy)phenyl)dipyrromethane

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