1-(3-Chlorophenyl)-2-fluoroethanamine

Base Information

• Chemical Name: 1-(3-Chlorophenyl)-2-fluoroethanamine
• CAS No.: 929972-34-9
• Molecular Formula: C₈H₉ClFN
• Molecular Weight: 173.618
• Mol file: 929972-34-9.mol

Synonyms:1-(3-CHLOROPHENYL)-2-FLUOROETHANAMINE;Benzenemethanamine, 3-chloro-α-(fluoromethyl)-

Chemical Property of 1-(3-Chlorophenyl)-2-fluoroethanamine

Chemical Property:

• PSA: 26.02000
• LogP: 3.81160

Purity/Quality:

1-(3-CHLOROPHENYL)-2-FLUOROETHANAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(3-Chlorophenyl)-2-fluoroethanamine

There total 11 articles about 1-(3-Chlorophenyl)-2-fluoroethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-(3-chlorophenyl)-2-fluoroethanone (90221-70-8) → 1-(3-chlorophenyl)-2-fluoroethanamine (929972-34-9)

Guidance literature:

1-(3-chlorophenyl)-2-fluoroethanone; With titanium(IV) isopropylate; ammonia; In ethanol; at 20 ℃; for 16h; Inert atmosphere;

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 5h;

Reference yield: 86.0%

rac-tert-butyl [1-(3-chlorophenyl)-2-fluoroethyl]carbamate → 1-(3-chlorophenyl)-2-fluoroethanamine (929972-34-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 60h;

Reference yield: 86.0%

tert-butyl [1-(3-chlorophenyl)-2-fluoroethyl]carbamate → 1-(3-chlorophenyl)-2-fluoroethanamine (929972-34-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; water; at 20 ℃; for 60h;

upstream raw materials:

2-bromo-1-(3-chloro-phenyl)-ethanone

1-(3-chlorophenyl)-2-fluoroethanone

3'-Chloroacetophenone

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