1,4-Endo-o-phenylenenaphthalene, 1,2,3,4-tetrahydro-

Base Information

• Chemical Name: 1,4-Endo-o-phenylenenaphthalene, 1,2,3,4-tetrahydro-
• CAS No.: 5675-64-9
• Molecular Formula: C16H14
• Molecular Weight: 206.287
• Hs Code.: 2906290090
• Mol file: 5675-64-9.mol

Synonyms:1,4-Endo-o-phenylenenaphthalene,1,2,3,4-tetrahydro-; 9,10-Dihydro-9,10-ethanoanthracene;Dibenzobicyclo[2.2.2]octadiene; NSC 155525

Chemical Property of 1,4-Endo-o-phenylenenaphthalene, 1,2,3,4-tetrahydro-

Chemical Property:

• Vapor Pressure: 0.000324mmHg at 25°C
• Boiling Point: 330.2°Cat760mmHg
• Flash Point: 161.4°C
• PSA: 0.00000
• Density: 1.129g/cm³
• LogP: 4.05760

Purity/Quality:

tetracyclo[6.6.2.0.0]hexadeca-2(7),3,5,9(14),10,12-hexaene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,4-Endo-o-phenylenenaphthalene, 1,2,3,4-tetrahydro-

There total 34 articles about 1,4-Endo-o-phenylenenaphthalene, 1,2,3,4-tetrahydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

<2,3:5,6>dibenzo<2.2.2>octa-2,5,7-triene (2734-13-6) → <2,3:5,6>dibenzo<2.2.2>octa-2,5-diene (5675-64-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; under 760 Torr;

DOI:10.1107/S010827019801275X

Reference yield: 94.0%

C22H18O2S (73301-18-5) → 9,10-ethanoanthracene (5675-64-9)

Guidance literature:

With sodium amalgam; Na₂HPO₄ buffer; In methanol; at -20 ℃;

DOI:10.1021/ja00522a075

Reference yield: 94.0%

C22H20O2S → 9,10-ethanoanthracene (5675-64-9)

Guidance literature:

With disodium hydrogenphosphate; sodium amalgam; In tetrahydrofuran; methanol; for 11h;

DOI:10.1021/jo00173a039

upstream raw materials:

ethene

anthracene

9,10-dihydro-9,10-etheno-anthracene

11-chloro-9,10-dihydro-9,10-ethenoanthracene

Downstream raw materials:

ethene

anthracene

2-(acetylamino)anthracene