(1S,3aR,7aR)-1-((S)-1-(3-hydroxy-3-Methylbutoxy)ethyl)-7a-Methylhexahydro-1H-inden-4(2H)-one

Base Information

Chemical Name:(1S,3aR,7aR)-1-((S)-1-(3-hydroxy-3-Methylbutoxy)ethyl)-7a-Methylhexahydro-1H-inden-4(2H)-one
CAS No.:884488-07-7
Molecular Formula:C17H30O3
Molecular Weight:282.42
Hs Code.:
Mol file:884488-07-7.mol

Synonyms:(1S,3aR,7aR)-Octahydro-1-[(1S)-1-(3-hydroxy-3-methylbutoxy)ethyl]-7a-methyl-4H-inden-4-one;(1S,3aR,7aR)-1-((S)-1-(3-hydroxy-3-Methylbutoxy)ethyl)-7a-Methylhexahydro-1H-inden-4(2H)-one;4H-Inden-4-one, octahydro-1-[(1S)-1-(3-hydroxy-3-methylbutoxy)ethyl]-7a-methyl-, (1S,3aR,7aR)-;(1S,3aR,7aR)-1-[(1S)-1-(3-hydroxy-3-methylbutoxy)ethyl]-7a-methyl-2,3,3a,5,6,7-hexahydro-1H-inden-4-one

Suppliers and Price of (1S,3aR,7aR)-1-((S)-1-(3-hydroxy-3-Methylbutoxy)ethyl)-7a-Methylhexahydro-1H-inden-4(2H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of (1S,3aR,7aR)-1-((S)-1-(3-hydroxy-3-Methylbutoxy)ethyl)-7a-Methylhexahydro-1H-inden-4(2H)-one

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (1S,3aR,7aR)-1-((S)-1-(3-hydroxy-3-Methylbutoxy)ethyl)-7a-Methylhexahydro-1H-inden-4(2H)-one

There total 14 articles about (1S,3aR,7aR)-1-((S)-1-(3-hydroxy-3-Methylbutoxy)ethyl)-7a-Methylhexahydro-1H-inden-4(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 192573-37-8
(20S)-de-A,B-22-oxacholestane-8β,25-diol

: 884488-07-7
(20S)-de-A,B-25-hydroxy-22-oxacholestan-8-one

Guidance literature:: With tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2006.01.061

Reference yield:

: 66774-80-9,111924-49-3
(S)-2-((3R,3aR,7S,7aR)-octahydro-7-hydroxy-3a-methyl-1H-inden-3-yl)propyl 4-methylbenzenesulfonate

: 884488-07-7
(20S)-de-A,B-25-hydroxy-22-oxacholestan-8-one

Guidance literature:: Multi-step reaction with 9 steps

1: 83 percent / imidazole

2: 85 percent / NaHCO₃, DMSO

3: 82 percent / O₂, t-BuOK / 2-methyl-propan-2-ol / Ambient temperature

4: K / propan-2-ol / Heating

5: 85 percent / N-methylmorpholine / benzene / 12 h / Ambient temperature

6: 80 percent / H₂ / Pd-C / ethanol

7: 80 percent / diethyl ether

8: 91 percent / HF / acetonitrile

9: PCC / CH₂Cl₂ / Ambient temperature

With 4-methyl-morpholine; 1H-imidazole; hydrogen fluoride; potassium tert-butylate; hydrogen; oxygen; potassium; sodium hydrogencarbonate; dimethyl sulfoxide; pyridinium chlorochromate; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; isopropyl alcohol; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4039(97)01056-3

Reference yield:

: 64190-52-9
(8S,20S)-de-A,B-20-(hydroxymethyl)pregnan-8-ol

: 884488-07-7
(20S)-de-A,B-25-hydroxy-22-oxacholestan-8-one

Guidance literature:: Multi-step reaction with 10 steps

1: 95 percent / pyridine

2: 83 percent / imidazole

3: 85 percent / NaHCO₃, DMSO

4: 82 percent / O₂, t-BuOK / 2-methyl-propan-2-ol / Ambient temperature

5: K / propan-2-ol / Heating

6: 85 percent / N-methylmorpholine / benzene / 12 h / Ambient temperature

7: 80 percent / H₂ / Pd-C / ethanol

8: 80 percent / diethyl ether

9: 91 percent / HF / acetonitrile

10: PCC / CH₂Cl₂ / Ambient temperature

With 4-methyl-morpholine; 1H-imidazole; hydrogen fluoride; potassium tert-butylate; hydrogen; oxygen; potassium; sodium hydrogencarbonate; dimethyl sulfoxide; pyridinium chlorochromate; palladium on activated charcoal; In pyridine; diethyl ether; ethanol; dichloromethane; isopropyl alcohol; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4039(97)01056-3