cis-cyclohexane-1,3-diamine hydrochloride

Base Information

• Chemical Name: cis-cyclohexane-1,3-diamine hydrochloride
• CAS No.: 498532-32-4
• Molecular Formula: C6H14N2.2ClH
• Molecular Weight: 151
• Mol file: 498532-32-4.mol

Synonyms:(1R,3S)-cyclohexane-1,3-diamine,dihydrochloride;

Chemical Property of cis-cyclohexane-1,3-diamine hydrochloride

Chemical Property:

• Melting Point: >360 °C(Solv: ethanol, 95% (64-17-5))
• PSA: 52.04000
• LogP: 3.21960
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

(1R,3S)-Cyclohexane-1,3-diaminedihydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of cis-cyclohexane-1,3-diamine hydrochloride

There total 2 articles about cis-cyclohexane-1,3-diamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-diaminocyclohexane (3385-21-5,26772-34-9,26883-70-5,115092-57-4) → C6H14N2*2ClH (498532-32-4)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol / 12 h / 25 °C

2: hydrogenchloride / water / 4 h / 70 - 80 °C

With hydrogenchloride; In methanol; water;

Reference yield:

1,3-diaminocyclohexane (3385-21-5,26772-34-9,26883-70-5,115092-57-4) → cis-cyclohexane-1,3-diamine dihydrochloride (28294-92-0,32175-26-1,498532-32-4)

Guidance literature:

Multi-step reaction with 2 steps

1: nickel(II) chloride hexahydrate

2: hydrogenchloride

With hydrogenchloride; nickel(II) chloride hexahydrate;

DOI:10.1016/j.bmcl.2013.09.016

Reference yield: 49.0%

C6H14N2*2ClH (498532-32-4) + benzyl chloroformate (501-53-1,94274-21-2) → benzyl cis-3-(aminocyclohexyl)carbamate (1223158-00-6,1261225-45-9)

Guidance literature:

With sodium hydrogencarbonate; In 1,4-dioxane; ethanol; water; at 0 ℃; for 2h; Concentration;

upstream raw materials:

1,3-diaminocyclohexane

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