Trans-4-(Trans-4-Pentylcyclohexyl)Cyclohexylmethanol

Base Information

• Chemical Name: Trans-4-(Trans-4-Pentylcyclohexyl)Cyclohexylmethanol
• CAS No.: 82598-08-1
• Molecular Formula: C₁₈H₃₄O
• Molecular Weight: 266.467
• Mol file: 82598-08-1.mol

Synonyms:Trans-4-(Trans-4-Pentylcyclohexyl)Cyclohexylmethanol;(trans,trans)-4'-pentyl-[1,1'-Bicyclohexyl]-4-methanol

Chemical Property of Trans-4-(Trans-4-Pentylcyclohexyl)Cyclohexylmethanol

Chemical Property:

• Melting Point: 130 °C
• PSA: 20.23000
• LogP: 5.17180
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: soluble in Methanol

Purity/Quality:

99.50% ^*data from raw suppliers

trans,trans-4'-Pentyl-4-bicyclohexylmethanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Trans-4-(Trans-4-Pentylcyclohexyl)Cyclohexylmethanol

There total 3 articles about Trans-4-(Trans-4-Pentylcyclohexyl)Cyclohexylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-4'-pentylbicyclohexyl-trans-4-carboxylic acid methylester (88416-73-3) → 4-n-pentyl-trans,trans-bicyclohexyl-4'-carbinol (82598-08-1)

Guidance literature:

trans-4'-pentylbicyclohexyl-trans-4-carboxylic acid methylester; With lithium aluminium tetrahydride; In tetrahydrofuran; at 3 - 10 ℃;

With ammonia; water; In tetrahydrofuran; ethyl acetate; Cooling with ice;

Reference yield:

trans-4-cyclohexyl-1-carboxylic acid (65355-33-1) → 4-n-pentyl-trans,trans-bicyclohexyl-4'-carbinol (82598-08-1)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 1h; Heating;

DOI:10.1002/hlca.19840670407

Reference yield:

4-n-pentyl-trans,trans-bicyclohexyl-4'-carbonitrile (65355-36-4) → 4-n-pentyl-trans,trans-bicyclohexyl-4'-carbinol (82598-08-1)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. H₂SO₄ / 5 h / Heating

2: lithium aluminum hydride / tetrahydrofuran / Ambient temperature

With lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran;

upstream raw materials:

trans-4-cyclohexyl-1-carboxylic acid

4-n-pentyl-trans,trans-bicyclohexyl-4'-carbonitrile

trans-4'-pentylbicyclohexyl-trans-4-carboxylic acid methylester

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