Technology Process of Benzoic acid, 2-hydroxy-, 3-chlorophenyl ester
There total 3 articles about Benzoic acid, 2-hydroxy-, 3-chlorophenyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonium peroxydisulfate; cerium(III) chloride; sodium hydrogencarbonate;
In
ethyl acetate;
at 35 ℃;
for 24h;
Irradiation;
DOI:10.1039/d1ra04130d
- Guidance literature:
-
With
2-pentafluorophenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; 1,4-diaza-bicyclo[2.2.2]octane; oxygen; sodium iodide; 9-(2-mesityl)-10-methylacridinium perchlorate;
In
dichloromethane;
at 20 ℃;
for 36h;
Schlenk technique;
Irradiation;
DOI:10.1039/c9cc09272b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene; pyridine; copper; copper(l) iodide / N,N-dimethyl-formamide / 160 °C / Inert atmosphere
2: silver nitrate; dipotassium peroxodisulfate; potassium trifluoroacetate / acetonitrile / 36 h / 130 °C / Sealed tube; Inert atmosphere
With
pyridine; dipotassium peroxodisulfate; copper(l) iodide; potassium trifluoroacetate; copper; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
N,N-dimethyl-formamide; acetonitrile;
2: |Smiles Aromatic Rearrangement;
DOI:10.1039/c6ob01758d
