4-BroMo-6-chloro-dibenzothiophene

Base Information

Chemical Name:4-BroMo-6-chloro-dibenzothiophene
CAS No.:1332939-29-3
Molecular Formula:C12H6BrClS
Molecular Weight:297.603
Hs Code.:
Mol file:1332939-29-3.mol

Synonyms:4-BroMo-6-chloro-dibenzothiophene;Dibenzothiophene, 4-bromo-6-chloro-;4-bromo-6-chlorodibenzo[b,d]thiophene;2-bromo-8-chlorodibenzo[b,d]thiophene

Suppliers and Price of 4-BroMo-6-chloro-dibenzothiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 4-BroMo-6-chloro-dibenzothiophene

Chemical Property:

Melting Point:165 - 167 °C (ethanol)
PSA：28.24000
LogP:5.47040

Purity/Quality:: HPLC≥98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-BroMo-6-chloro-dibenzothiophene

There total 9 articles about 4-BroMo-6-chloro-dibenzothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1332939-75-9
3-bromo-2',3'-dichloro-[1,1'-biphenyl]-2-thiol

: 1332939-29-3
4-bromo-6-chlorodibenzo[b,d]thiophene

Guidance literature:: With caesium carbonate; In acetonitrile; at 130 ℃; for 0.166667h; Microwave irradiation;
DOI:10.1039/c1ob05282a

Reference yield: 40.0%

: C₁₄H₁₂BrClOS

: 1332939-25-9
6-bromo-2-chlorodibenzo[b,d]thiophene

: 1332939-29-3
4-bromo-6-chlorodibenzo[b,d]thiophene

Guidance literature:: C₁₄H₁₂BrClOS; With trifluorormethanesulfonic acid; at 20 ℃; for 24h;

With pyridine; In water; for 0.5h; Reflux;

Reference yield:

: 1332939-53-3
3-bromo-2',3'-dichloro-[1,1'-biphenyl]-2-amine

: 1332939-29-3
4-bromo-6-chlorodibenzo[b,d]thiophene

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / methanol / 0.17 h / 0 °C

1.2: 0 °C

1.3: 0 - 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

3.1: caesium carbonate / acetonitrile / 0.17 h / 130 °C / Microwave irradiation

With hydrogenchloride; lithium aluminium tetrahydride; caesium carbonate; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1039/c1ob05282a