Glucosyringic acid

Base Information

Chemical Name:Glucosyringic acid
CAS No.:33228-65-8
Molecular Formula:C₁₅H₂₀O₁₀
Molecular Weight:360.318
Hs Code.:
DSSTox Substance ID:DTXSID20186870
Nikkaji Number:J18.842E
Wikidata:Q72480470
ChEMBL ID:CHEMBL5082798
Mol file:33228-65-8.mol

Synonyms:gluco-syringic acid;glucosyringic acid

Suppliers and Price of Glucosyringic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
Glucosyringicacid
5mg
$ 463.00

Total 18 raw suppliers

Chemical Property of Glucosyringic acid

Chemical Property:

Melting Point:212 °C (decomp)
Boiling Point:611.1±55.0 °C(Predicted)
PKA:4.11±0.10(Predicted)
PSA：155.14000
Density:1.519±0.06 g/cm3(Predicted)
LogP:-1.41930
XLogP3:-1
Hydrogen Bond Donor Count:5
Hydrogen Bond Acceptor Count:10
Rotatable Bond Count:6
Exact Mass:360.10564683
Heavy Atom Count:25
Complexity:432

Purity/Quality:

HPLC≥95% ^*data from raw suppliers

Glucosyringicacid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=CC(=C1OC2C(C(C(C(O2)CO)O)O)O)OC)C(=O)O
Isomeric SMILES:COC1=CC(=CC(=C1O[C@H]2[C@@H]([C@H]([C@@H]([C@H](O2)CO)O)O)O)OC)C(=O)O

Technology Process of Glucosyringic acid

There total 5 articles about Glucosyringic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 119643-01-5
(2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-(2,6-dimethoxy-4-(methoxycarbonyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 33228-65-8,141243-28-9
glucosyringic acid

Guidance literature:: With water; potassium hydroxide; In methanol; at 0 - 20 ℃; for 16h;

Reference yield: 75.0%

: 34992-99-9
3,5-dimethoxy-4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)benzoic acid

: 33228-65-8,141243-28-9
glucosyringic acid

Guidance literature:: With sodium methylate; In acetic acid; for 5h; Ambient temperature;
DOI:10.1016/0008-6215(90)84294-5

Reference yield:

: 3947-62-4,6207-76-7,19235-21-3,22554-70-7,22860-22-6,47339-09-3,57884-82-9,62057-79-8,70191-05-8,109525-54-4,140147-37-1,10343-06-3
2,3,4,5-tetra-O-acetyl-D-glucopyranose

: 33228-65-8,141243-28-9
glucosyringic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0 °C / Inert atmosphere

2.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

2.2: 2.25 h / -40 - 0 °C / Inert atmosphere; Molecular sieve

3.1: potassium hydroxide; water / methanol / 16 h / 0 - 20 °C

With water; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium hydroxide; In methanol; dichloromethane;