12-(naphthaleN-2yl)benoza[a]athracene

Base Information

Chemical Name:12-(naphthaleN-2yl)benoza[a]athracene
CAS No.:116027-92-0
Molecular Formula:C28H18
Molecular Weight:354.44
Hs Code.:
Mol file:116027-92-0.mol

Synonyms:12-[2]naphthyl-benz[a]anthracene;12-[2]Naphthyl-benz[a]anthracen;12-Naphthalen-2-yl-benzo[a]anthracene;

Suppliers and Price of 12-(naphthaleN-2yl)benoza[a]athracene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 11 raw suppliers

Chemical Property of 12-(naphthaleN-2yl)benoza[a]athracene

Chemical Property:

PSA：0.00000
LogP:7.96640

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 12-(naphthaleN-2yl)benoza[a]athracene

There total 4 articles about 12-(naphthaleN-2yl)benoza[a]athracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: acetic acid {2-[acetoxy-(naphthalen-2-yl)-methyl]phenyl}-(naphthalen-2-yl)-methyl ester

: 116027-92-0
12-naphthalen-2-yl-benzo[a]anthracene

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; for 0.0166667h;
DOI:10.1021/jo7017334

Reference yield:

: 115916-89-7
[2]naphthyl-(2-[2]naphthylmethyl-phenyl)-ketone

: 116027-92-0
12-naphthalen-2-yl-benzo[a]anthracene

Guidance literature:: With hydrogen bromide; acetic acid; at 180 ℃;
DOI:10.1021/ja01540a051

Reference yield:

: 580-13-2
2-bromonaphthalene

: 116027-92-0
12-naphthalen-2-yl-benzo[a]anthracene

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / 30 h / -78 °C / Inert atmosphere

1.2: 15 h / -78 - 20 °C / Inert atmosphere

2.1: triethylamine; dmap / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

3.1: methanesulfonic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

With dmap; n-butyllithium; methanesulfonic acid; triethylamine; In tetrahydrofuran; dichloromethane;