Carbamic acid, (3-cyano-1-methylpropyl)-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, (3-cyano-1-methylpropyl)-, 1,1-dimethylethyl ester (9CI)
CAS No.:172833-24-8
Molecular Formula:C₁₀H₁₈N₂O₂
Molecular Weight:198.265
Hs Code.:
Mol file:172833-24-8.mol

Synonyms:Carbamic acid, (3-cyano-1-methylpropyl)-, 1,1-dimethylethyl ester (9CI)

Suppliers and Price of Carbamic acid, (3-cyano-1-methylpropyl)-, 1,1-dimethylethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
Tert-butylN-(4-cyanobutan-2-yl)carbamate
10g
$ 2997.00

AK Scientific
Tert-butylN-(4-cyanobutan-2-yl)carbamate
5g
$ 2053.00

Total 2 raw suppliers

Chemical Property of Carbamic acid, (3-cyano-1-methylpropyl)-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

Boiling Point:329.0±25.0 °C(Predicted)
PKA:12.19±0.46(Predicted)
PSA：62.12000
Density:0.992±0.06 g/cm3(Predicted)
LogP:2.59428

Purity/Quality:

98% ^*data from raw suppliers

Tert-butylN-(4-cyanobutan-2-yl)carbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, (3-cyano-1-methylpropyl)-, 1,1-dimethylethyl ester (9CI)

There total 1 articles about Carbamic acid, (3-cyano-1-methylpropyl)-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.2%

: 773837-37-9
sodium cyanide

: 98082-30-5
3-[N-(tert-butyloxycarbonyl)]amino-1-butyl methanesulfonate

: 172833-24-8
4-[N-(tert-butyloxycarbonyl)]-aminovaleronitrile

Guidance literature:: In dimethyl sulfoxide; at 45 ℃; for 8h;
DOI:10.1021/jm200293r

Reference yield: 75.0%

: 172833-24-8
4-[N-(tert-butyloxycarbonyl)]-aminovaleronitrile

: 172833-25-9
4-[N-(tert-butyloxycarbonyl)]-1,4-diaminopentane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at -10 - -5 ℃; for 1.33h;
DOI:10.1021/jm200293r

Reference yield:

: 172833-24-8
4-[N-(tert-butyloxycarbonyl)]-aminovaleronitrile

: 1-(N-o-nitrophenylsulfonyl)amino-4-(N-tert-butyloxycarbonyl)aminopentane

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / diethyl ether / 1.33 h / -10 - -5 °C

2: triethylamine / dichloromethane / 4.5 h / 0 - 20 °C

With lithium aluminium tetrahydride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1021/jm200293r