4-CHLORO-1-(3-CHLOROPHENYL)-1-OXOBUTANE

Base Information

• Chemical Name: 4-CHLORO-1-(3-CHLOROPHENYL)-1-OXOBUTANE
• CAS No.: 90793-58-1
• Molecular Formula: C10H10Cl2O
• Molecular Weight: 217.095
• Hs Code.: 2914700090
• Mol file: 90793-58-1.mol

Synonyms:4-CHLORO-1-(3-CHLOROPHENYL)-1-OXOBUTANE

Chemical Property of 4-CHLORO-1-(3-CHLOROPHENYL)-1-OXOBUTANE

Chemical Property:

• Vapor Pressure: 0.000149mmHg at 25°C
• Boiling Point: 332.1°C at 760 mmHg
• Flash Point: 140°C
• PSA: 17.07000
• Density: 1.224g/cm³
• LogP: 3.54170

Purity/Quality:

97% ^*data from raw suppliers

4-Chloro-1-(3-chlorophenyl)-1-oxobutane 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-CHLORO-1-(3-CHLOROPHENYL)-1-OXOBUTANE

There total 2 articles about 4-CHLORO-1-(3-CHLOROPHENYL)-1-OXOBUTANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-(3-chlorophenyl)cyclobutanol → 4-chloro-1-(3-chlorophenyl)butan-1-one (90793-58-1)

Guidance literature:

With 1,10-Phenanthroline; tert-butylhypochlorite; silver trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 6h; regioselective reaction; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.orglett.5b03649

Reference yield:

→ 4-chloro-1-(3-chlorophenyl)butan-1-one (90793-58-1)

Guidance literature:

m-Chlorphenylmagnesiumbromid, Cl-(CH2)3-CN;

Refernces