Carbamic acid, [(methylnitroamino)methylene]-, ethyl ester (9CI)

Base Information

• Chemical Name: Carbamic acid, [(methylnitroamino)methylene]-, ethyl ester (9CI)
• CAS No.: 212265-02-6
• Molecular Formula: C₅H₉N₃O₄
• Molecular Weight: 175.144
• Mol file: 212265-02-6.mol

Synonyms:Carbamic acid, [(methylnitroamino)methylene]-, ethyl ester (9CI)

Chemical Property of Carbamic acid, [(methylnitroamino)methylene]-, ethyl ester (9CI)

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Technology Process of Carbamic acid, [(methylnitroamino)methylene]-, ethyl ester (9CI)

There total 3 articles about Carbamic acid, [(methylnitroamino)methylene]-, ethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

methylnitroamine (598-57-2) + ethoxymethylene urethane (18804-89-2) → N2-Ethoxycarbonyl-N1-methyl-N1-nitroformamidine (212265-02-6)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 120 - 125 ℃; for 3h;

Reference yield: 33.0%

methylnitroamine (598-57-2) + N-(Carboaethoxy-imino-methyl)-urethan (18804-90-5) → Tris-(aethoxycarbonylamino)-methan (18804-87-0) + N2-Ethoxycarbonyl-N1-methyl-N1-nitroformamidine (212265-02-6)

Guidance literature:

In toluene; Yields of byproduct given; 1.) 70-80 deg C, 8 h, 2.) 20 deg C, 16 h;

Reference yield: 27.0%

methylnitroamine (598-57-2) + orthoformic acid triethyl ester (122-51-0) + urethane (51-79-6) → N2-Ethoxycarbonyl-N1-methyl-N1-nitroformamidine (212265-02-6)

Guidance literature:

In toluene; 1.) 120-125 deg C, 6 h, 2.) 20 deg C, 16 h;

upstream raw materials:

methylnitroamine

ethoxymethylene urethane

N-(Carboaethoxy-imino-methyl)-urethan

orthoformic acid triethyl ester

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