Cyclobutaneacetaldehyde, 3-formyl-2,2-dimethyl-, (1S,3S)- (9CI)

Base Information

Chemical Name:Cyclobutaneacetaldehyde, 3-formyl-2,2-dimethyl-, (1S,3S)- (9CI)
CAS No.:208651-69-8
Molecular Formula:C₉H₁₄O₂
Molecular Weight:154.209
Hs Code.:
Mol file:208651-69-8.mol

Synonyms:Cyclobutaneacetaldehyde, 3-formyl-2,2-dimethyl-, (1S,3S)- (9CI)

Suppliers and Price of Cyclobutaneacetaldehyde, 3-formyl-2,2-dimethyl-, (1S,3S)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclobutaneacetaldehyde, 3-formyl-2,2-dimethyl-, (1S,3S)- (9CI)

Chemical Property:

PSA：34.14000
LogP:1.43660

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cyclobutaneacetaldehyde, 3-formyl-2,2-dimethyl-, (1S,3S)- (9CI)

There total 4 articles about Cyclobutaneacetaldehyde, 3-formyl-2,2-dimethyl-, (1S,3S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 208651-73-4
2-((1S,3S)-3-Hydroxymethyl-2,2-dimethyl-cyclobutyl)-ethanol

: 208651-69-8,552810-14-7
(1S,3S)-2,2-Dimethyl-3-(2-oxo-ethyl)-cyclobutanecarbaldehyde

Guidance literature:: With oxalyl dichloride; TEA; dimethyl sulfoxide; at -60 ℃;
DOI:10.1016/S0040-4039(98)00557-7

Reference yield:

: 64396-97-0
(+)-cis-pinonic acid

: 208651-69-8,552810-14-7
(1S,3S)-2,2-Dimethyl-3-(2-oxo-ethyl)-cyclobutanecarbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: NaOBr / dioxane; H₂O / 0 °C

2: 95 percent / diethyl ether

3: 90 percent / LiBH₄ / tetrahydrofuran / 4 h / Heating

4: (COCl)2, DMSO, TEA / -60 °C

With lithium borohydride; sodium hypobromide; oxalyl dichloride; TEA; dimethyl sulfoxide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; water;
DOI:10.1016/S0040-4039(98)00557-7

Reference yield:

: 208651-71-2
cis-2,2-dimethyl-3-carboxycyclobutylethanoic acid

: 208651-69-8,552810-14-7
(1S,3S)-2,2-Dimethyl-3-(2-oxo-ethyl)-cyclobutanecarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / diethyl ether

2: 90 percent / LiBH₄ / tetrahydrofuran / 4 h / Heating

3: (COCl)2, DMSO, TEA / -60 °C

With lithium borohydride; oxalyl dichloride; TEA; dimethyl sulfoxide; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4039(98)00557-7