3,3,6,8-tetrachloro-7-methoxy-1H-quinoline-2,4-dione

Base Information

Chemical Name:3,3,6,8-tetrachloro-7-methoxy-1H-quinoline-2,4-dione
CAS No.:102249-22-9
Molecular Formula:C₁₀H₅Cl₄NO₃
Molecular Weight:328.967
Hs Code.:
DSSTox Substance ID:DTXSID50356504
Wikidata:Q82135865
Mol file:102249-22-9.mol

Synonyms:3,3,6,8-tetrachloro-7-methoxy-1H-quinoline-2,4-dione;102249-22-9;3,3,6,8-tetrachloro-7-methoxy-2,4(1H,3H)-quinolinedione;AE-406/41057134;DTXSID50356504

Suppliers and Price of 3,3,6,8-tetrachloro-7-methoxy-1H-quinoline-2,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 3,3,6,8-tetrachloro-7-methoxy-1H-quinoline-2,4-dione

Chemical Property:

Vapor Pressure:1.98E-10mmHg at 25°C
Boiling Point:507.7°Cat760mmHg
Flash Point:260.9°C
Density:1.73g/cm³
XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:328.899404
Heavy Atom Count:18
Complexity:389

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C2C(=C1Cl)NC(=O)C(C2=O)(Cl)Cl)Cl

Technology Process of 3,3,6,8-tetrachloro-7-methoxy-1H-quinoline-2,4-dione

There total 2 articles about 3,3,6,8-tetrachloro-7-methoxy-1H-quinoline-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 27037-34-9
4-hydroxy-7-methoxy-2-oxo-1,2-dihydroquinoline

: 102249-21-8
7-methoxy-3,3,6-trichloro-2,4-dioxo-1,2,3,4-tetrahydroquinoline

: 102249-22-9
7-methoxy-3,3,6,8-tetrachloro-2,4-dioxo-1,2,3,4-tetrahydroquinoline

Guidance literature:: With sulfuryl dichloride; In 1,4-dioxane;
DOI:10.1002/jhet.5570220431

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 102249-22-9
7-methoxy-3,3,6,8-tetrachloro-2,4-dioxo-1,2,3,4-tetrahydroquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / POCl₃ / 95 °C

2: 27 percent / sulfuryl chloride / dioxane

With sulfuryl dichloride; trichlorophosphate; In 1,4-dioxane;
DOI:10.1002/jhet.5570220431