(3-Methoxy-3-methylbutyl)amine

Base Information

• Chemical Name: (3-Methoxy-3-methylbutyl)amine
• CAS No.: 1268153-93-0
• Molecular Formula: C₆H₁₅NO
• Molecular Weight: 117.191
• Hs Code.: 2922199090
• Mol file: 1268153-93-0.mol

Synonyms:(3-Methoxy-3-methylbutyl)amine;(3-Methoxy-3-Methylbutyl)aMine (SALTDATA: FREE);3-methoxy-3-methyl-butan-1-amine;3-methoxy-3-methylbutan-1-amine

Chemical Property of (3-Methoxy-3-methylbutyl)amine

Chemical Property:

• PSA: 35.25000
• LogP: 1.46050

Purity/Quality:

97% ^*data from raw suppliers

(3-methoxy-3-methylbutyl)amine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-Methoxy-3-methylbutyl)amine

There total 3 articles about (3-Methoxy-3-methylbutyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

1-azido-3-methoxy-3-methylbutane → 3-methoxy-3-methylbutan-1-amine (1268153-93-0)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 16h;

Reference yield:

solfit (56539-66-3) → 3-methoxy-3-methylbutan-1-amine (1268153-93-0)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / 16 h / 0 - 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 20 °C

With pyridine; sodium azide; palladium 10% on activated carbon; hydrogen; In ethanol; N,N-dimethyl-formamide;

Reference yield:

3-methoxy-3-methylbutyl 4-methylbenzenesulfonate (869370-01-4) → 3-methoxy-3-methylbutan-1-amine (1268153-93-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 20 °C

With sodium azide; palladium 10% on activated carbon; hydrogen; In ethanol; N,N-dimethyl-formamide;

upstream raw materials:

solfit

3-methoxy-3-methylbutyl 4-methylbenzenesulfonate