9-beta-d-Arabinofuranosyl-9H-purine-6-thiol triacetate ester

Base Information

• Chemical Name: 9-beta-d-Arabinofuranosyl-9H-purine-6-thiol triacetate ester
• CAS No.: 98028-94-5
• Molecular Formula: C₁₆H₁₈N₄O₇S
• Molecular Weight: 410.408
• Mol file: 98028-94-5.mol

Synonyms:9-beta-d-Arabinofuranosyl-9H-purine-6-thiol triacetate ester

Chemical Property of 9-beta-d-Arabinofuranosyl-9H-purine-6-thiol triacetate ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 9-beta-d-Arabinofuranosyl-9H-purine-6-thiol triacetate ester

There total 2 articles about 9-beta-d-Arabinofuranosyl-9H-purine-6-thiol triacetate ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2',3',5'-tri-O-acetylinosine (3181-38-2) → 6-mercapto-(2',3',5'-tri-O-acetyl)purine (7687-42-5,98028-94-5)

Guidance literature:

With tetraphosphorus decasulfide; In toluene; at 80 ℃; for 2h; Time; Large scale;

Reference yield:

Inosine (58-63-9) → 6-mercapto-(2',3',5'-tri-O-acetyl)purine (7687-42-5,98028-94-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 2 h / 60 °C / Large scale

2: tetraphosphorus decasulfide / toluene / 2 h / 80 °C / Large scale

With tetraphosphorus decasulfide; In toluene;

upstream raw materials:

2',3',5'-tri-O-acetylinosine

Inosine

Refernces