2-chloro-3-methylbenzenemethanamine

Base Information

Chemical Name:2-chloro-3-methylbenzenemethanamine
CAS No.:1044256-78-1
Molecular Formula:C₈H₁₀ClN
Molecular Weight:155.627
Hs Code.:
Mol file:1044256-78-1.mol

Synonyms:2-chloro-3-methylbenzenemethanamine

Suppliers and Price of 2-chloro-3-methylbenzenemethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-chloro-3-methylbenzenemethanamine

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-chloro-3-methylbenzenemethanamine

There total 4 articles about 2-chloro-3-methylbenzenemethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 134271-45-7
1-(bromomethyl)-2-chloro-3-methylbenzene

: 1044256-78-1
(2-chloro-3-methylphenyl)methanamine

Guidance literature:: 1-(bromomethyl)-2-chloro-3-methylbenzene; With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; for 14h;

With triphenylphosphine; In tetrahydrofuran; water; for 72h;

Reference yield:

: 1044256-77-0
1-Azidomethyl-2-chloro-3-methyl-benzene

: 1044256-78-1
(2-chloro-3-methylphenyl)methanamine

Guidance literature:: With potassium hydroxide; triphenylphosphine; In tetrahydrofuran; water; for 14h; Alkaline aqueous solution;

Reference yield:

: 6781-98-2
2,6-dimethyl-1-chlorobenzene

: 1044256-78-1
(2-chloro-3-methylphenyl)methanamine

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide / dibenzoyl peroxide / tetrachloromethane / 1 h / Heating / reflux

2: sodium azide / dimethyl sulfoxide / 14 h / 55 °C

3: potassium hydroxide; triphenylphosphine / tetrahydrofuran; water / 14 h / Alkaline aqueous solution

With potassium hydroxide; N-Bromosuccinimide; sodium azide; triphenylphosphine; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; water; dimethyl sulfoxide;