Tert-butyl 3-nitropiperidine-1-carboxylate

Base Information

Chemical Name:Tert-butyl 3-nitropiperidine-1-carboxylate
CAS No.:1313738-96-3
Molecular Formula:C₁₀H₁₈N₂O₄
Molecular Weight:230.264
Hs Code.:2933399090
European Community (EC) Number:839-123-7
DSSTox Substance ID:DTXSID30693520
Mol file:1313738-96-3.mol

Synonyms:tert-butyl 3-nitropiperidine-1-carboxylate;1313738-96-3;tert-butyl 3-Nitropiperidin-1-carboxylate;SCHEMBL19331841;DTXSID30693520;AMY24071;AKOS015907492;AKOS015949276;PB48099;PS-15725;tert-butyl3-nitropiperidine-1-carboxylate;FT-0685131;E87643;EN300-768689;3-Nitropiperidine-1-carboxylic acid tert-butyl ester;J-524561;W-205360

Suppliers and Price of Tert-butyl 3-nitropiperidine-1-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-butyl3-Nitropiperidine-1-carboxylate 95+%
1g
$ 585.00

Chemenu
tert-butyl3-Nitropiperidine-1-carboxylate 95%
1g
$ 553.00

Total 8 raw suppliers

Chemical Property of Tert-butyl 3-nitropiperidine-1-carboxylate

Chemical Property:

Boiling Point:327.7±31.0 °C(Predicted)
PKA:7.68±0.20(Predicted)
PSA：75.36000
Density:1.16±0.1 g/cm3(Predicted)
LogP:2.12370
XLogP3:1.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:230.12665706
Heavy Atom Count:16
Complexity:280

Purity/Quality:

99%, ^*data from raw suppliers

tert-butyl3-Nitropiperidine-1-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)N1CCCC(C1)[N+](=O)[O-]

Technology Process of Tert-butyl 3-nitropiperidine-1-carboxylate

There total 2 articles about Tert-butyl 3-nitropiperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl 3-hydroxyiminopiperidine-1-carboxylate

: 1313738-96-3
(±)-tert-butyl 3-nitropiperidine-1-carboxylate

Guidance literature:: With urea hydrogen peroxide adduct; sodium hydrogencarbonate; trifluoroacetic anhydride; In acetonitrile; at 0 - 80 ℃; for 2h;

Reference yield:

: 98977-36-7
3-oxo-piperidine-1-carboxylic acid tert-butyl ester

: 1313738-96-3
(±)-tert-butyl 3-nitropiperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; hydroxylamine hydrochloride / ethanol / 1 h / 90 °C

2: trifluoroacetic anhydride; urea hydrogen peroxide adduct; sodium hydrogencarbonate / acetonitrile / 2 h / 0 - 80 °C

With hydroxylamine hydrochloride; urea hydrogen peroxide adduct; sodium hydrogencarbonate; triethylamine; trifluoroacetic anhydride; In ethanol; acetonitrile;