4-chloro-2-[4-[(pyrrolidin-1-yl)carbonyl]piperidin-1-yl]benzaldehyde

Base Information

Chemical Name:4-chloro-2-[4-[(pyrrolidin-1-yl)carbonyl]piperidin-1-yl]benzaldehyde
CAS No.:1460032-48-7
Molecular Formula:C₁₇H₂₁ClN₂O₂
Molecular Weight:320.819
Hs Code.:
Mol file:1460032-48-7.mol

Synonyms:4-chloro-2-[4-[(pyrrolidin-1-yl)carbonyl]piperidin-1-yl]benzaldehyde

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Chemical Property of 4-chloro-2-[4-[(pyrrolidin-1-yl)carbonyl]piperidin-1-yl]benzaldehyde

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Technology Process of 4-chloro-2-[4-[(pyrrolidin-1-yl)carbonyl]piperidin-1-yl]benzaldehyde

There total 1 articles about 4-chloro-2-[4-[(pyrrolidin-1-yl)carbonyl]piperidin-1-yl]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 188979-07-9
4-[(pyrrolidin-1-yl)carbonyl]piperidine hydrochloride

: 61072-56-8
4-chloro-2-fluorobenzaldehyde

: 1460032-48-7
4-chloro-2-[4-[(pyrrolidin-1-yl)carbonyl]piperidin-1-yl]benzaldehyde

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 100 ℃;

Reference yield: 81.0%

: 1460032-48-7
4-chloro-2-[4-[(pyrrolidin-1-yl)carbonyl]piperidin-1-yl]benzaldehyde

: 57260-71-6
1-t-Butoxycarbonylpiperazine

: 1460032-53-4
tert-butyl 4-[(4-chloro-2-[4-[(pyrrolidin-1-yl)carbonyl]piperidin-1-yl]phenyl)methyl]piperazine-1-carboxylate

Guidance literature:: 4-chloro-2-[4-[(pyrrolidin-1-yl)carbonyl]piperidin-1-yl]benzaldehyde; 1-t-Butoxycarbonylpiperazine; In 1,2-dichloro-ethane; at 20 ℃; for 0.5h;

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃;

Reference yield:

: 1460032-48-7
4-chloro-2-[4-[(pyrrolidin-1-yl)carbonyl]piperidin-1-yl]benzaldehyde

: 1460032-56-7
1-[(4-chloro-2-[4-[(pyrrolidin-1-yl)carbonyl]piperidin-1-yl]phenyl)methyl]piperazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,2-dichloro-ethane / 0.5 h / 20 °C

1.2: 20 °C

2.1: trifluoroacetic acid / dichloromethane / 20 °C

With trifluoroacetic acid; In dichloromethane; 1,2-dichloro-ethane;