2,6-Dichloroanthracene

Base Information

• Chemical Name: 2,6-Dichloroanthracene
• CAS No.: 26154-35-8
• Molecular Formula: C14H8Cl2
• Molecular Weight: 247.12
• Hs Code.: 2903999090
• Mol file: 26154-35-8.mol

Synonyms:2,6-Dichloroanthracene

Chemical Property of 2,6-Dichloroanthracene

Chemical Property:

• PSA: 0.00000
• LogP: 5.29980

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,6-Dichloroanthracene

There total 6 articles about 2,6-Dichloroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

3,7-dichloro-10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-one (32668-90-9) → 2,6-Dichlor-anthracen (26154-35-8)

Guidance literature:

at 900 - 1000 ℃; for 2h; under 0.8 - 3.0002 Torr;

DOI:10.1021/jo00131a016

Reference yield: 40.0%

2,6-dichloro-9,10-anthraquinone (605-40-3) → 2,6-Dichlor-anthracen (26154-35-8)

Guidance literature:

With aluminium; mercury dichloride; In tetrachloromethane; cyclohexanol; for 48h; Reflux;

Reference yield:

disodium 9,10-anthraquinone-2,6-disulfonate (853-68-9) → 2,6-Dichlor-anthracen (26154-35-8)

Guidance literature:

Multi-step reaction with 2 steps

1: NaClO₃, HCl

2: Al cyclohexoxide / various solvent(s)

With hydrogenchloride; sodium chlorate; Al(c-C₆H₁₁O)3; In various solvent(s);

DOI:10.1016/S0040-4039(00)87868-5

upstream raw materials:

2,6-dichloro-9,10-anthraquinone

3,7-dichloro-10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-one

10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-one

3,7-dinitro-10,11-dihydro-5H-dibenzocyclohepten-5-one

Refernces

• 1、 Kawada, Yuzo,Okamoto, Yoshio,Iwamura, Hiizu. "CORRELATED INTERNAL ROTATION IN BIS(2,6-DICHLORO-9-TRIPTYCYL)METHANE. TO WHAT EXTENT CAN PHASE ISOMERS BE SEPARATED AND IDENTIFIED?". . p. 5359 - 5362. Retrieved 1983.