5-CHLORO-HEX-5-ENOIC ACID

Base Information

• Chemical Name: 5-CHLORO-HEX-5-ENOIC ACID
• CAS No.: 731773-27-6
• Molecular Formula: C₆H₉ClO₂
• Molecular Weight: 148.589
• Hs Code.: 2916190090
• Mol file: 731773-27-6.mol

Synonyms:5-CHLORO-HEX-5-ENOIC ACID;5-CHLORO-5-HEXENOIC ACID

Chemical Property of 5-CHLORO-HEX-5-ENOIC ACID

Chemical Property:

• Vapor Pressure: 0.00836mmHg at 25°C
• Boiling Point: 247.2°C at 760 mmHg
• PKA: 4.46±0.10(Predicted)
• Flash Point: 103.3°C
• PSA: 37.30000
• Density: 1.156g/cm³
• LogP: 1.99380

Purity/Quality:

98% ^*data from raw suppliers

5-Chloro-5-hexenoicacid 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-CHLORO-HEX-5-ENOIC ACID

There total 1 articles about 5-CHLORO-HEX-5-ENOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

hex-5-ynoic acid (53293-00-8) → 5-chlorohex-5-enoic acid (731773-27-6)

Guidance literature:

With hydrogenchloride; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; Au-TiO₂; In N,N-dimethyl-formamide; at 100 ℃; for 7h; regioselective reaction;

DOI:10.1021/acs.orglett.7b02101

upstream raw materials:

hex-5-ynoic acid