Ethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside

Base Information

Chemical Name:Ethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside
CAS No.:130539-43-4
Molecular Formula:C16H19NO6S
Molecular Weight:353.396
Hs Code.:
Mol file:130539-43-4.mol

Synonyms:Ethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside

Suppliers and Price of Ethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemenu
Ethyl2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside 97%
1g
$ 1197.00

Arctom
Ethyl2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside >97%
1g
$ 350.00

Arctom
Ethyl2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside >97%
5g
$ 995.00

Alichem
beta-D-Glucopyranoside,ethyl2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-
250mg
$ 566.10

Alichem
beta-D-Glucopyranoside,ethyl2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-
100mg
$ 345.60

Alichem
beta-D-Glucopyranoside,ethyl2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-
1g
$ 1305.60

AK Scientific
Ethyl2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside
5g
$ 1403.00

AK Scientific
Ethyl2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside
1g
$ 532.00

Total 22 raw suppliers

Chemical Property of Ethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside

Chemical Property:

Boiling Point:594.3±50.0 °C(Predicted)
PKA:13.00±0.70(Predicted)
PSA：132.60000
Density:1.52±0.1 g/cm3(Predicted)
LogP:-0.21880

Purity/Quality:

98% ^*data from raw suppliers

Ethyl2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Ethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside

There total 12 articles about Ethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-1-thio-beta-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 99409-32-2
ethyl-3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 130539-43-4
ethyl 2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 85-44-9
phthalic anhydride

: 130539-43-4
ethyl 2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / water / 24 h / 20 °C

2: pyridine

3: boron trifluoride diethyl etherate / chloroform / Reflux

4: methanol; sodium methylate

With pyridine; methanol; boron trifluoride diethyl etherate; sodium methylate; sodium hydroxide; In chloroform; water;
DOI:10.1016/j.carres.2011.05.024

Reference yield:

: 10022-13-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose

: 130539-43-4
ethyl 2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 62.5 percent / BF₃*Et₂O / CH₂Cl₂ / 22 h

2: 69.5 percent / sodium methoxide / methanol / 3 h

With boron trifluoride diethyl etherate; sodium methylate; In methanol; dichloromethane;
DOI:10.1081/CAR-120020480