Technology Process of (E)-9-(3-Furanyl)-2,6-dimethyl-2,5-nonadien-4-one
There total 9 articles about (E)-9-(3-Furanyl)-2,6-dimethyl-2,5-nonadien-4-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
methanol;
at 60 ℃;
for 3h;
DOI:10.1071/CH9802729
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 1.) mercuric acetate, water, 2.) sodium borohydride / 1.) water, THF, 7 min, 2.) 2 h
2: 63 percent / lithium, ammonia / tetrahydrofuran / 3 h / -33 °C
3: 1.4 g / pyridine / 15 h / Ambient temperature
4: 1.) thionyl chloride, pyridine, 2.) LAH / 1.) ether 0 deg C, 10 min
5: pyridine
6: LiAlH4
7: 35 percent / pyridinum chlorochromate / CH2Cl2 / 2 h
8: 50 percent / aq. NaOH / methanol / 3 h / 60 °C
With
pyridine; sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; thionyl chloride; mercury(II) diacetate; ammonia; water; lithium; pyridinium chlorochromate;
In
tetrahydrofuran; pyridine; methanol; dichloromethane;
DOI:10.1071/CH9802729
- Guidance literature:
-
Multi-step reaction with 3 steps
1: LiAlH4
2: 35 percent / pyridinum chlorochromate / CH2Cl2 / 2 h
3: 50 percent / aq. NaOH / methanol / 3 h / 60 °C
With
sodium hydroxide; lithium aluminium tetrahydride; pyridinium chlorochromate;
In
methanol; dichloromethane;
DOI:10.1071/CH9802729
