9-Tricosene

Base Information

• Chemical Name: 9-Tricosene
• CAS No.: 35857-62-6
• Molecular Formula: C23H46
• Molecular Weight: 322.618
• European Community (EC) Number: 609-184-2
• UNII: T192MHP98E
• DSSTox Substance ID: DTXSID6035734
• Nikkaji Number: J1.603.159C,J575.738J
• Wikidata: Q27289534
• Metabolomics Workbench ID: 5262
• Mol file: 35857-62-6.mol

Synonyms:9-Tricosene;(E)-9-Tricosene;trans-9-Tricosene;(E)-tricos-9-ene;35857-62-6;9-Tricosene, (9E)-;52078-48-5;Tech. Muscalure;9-Tricosene, (E)-;EPA Pesticide Chemical Code 103202;UNII-T192MHP98E;T192MHP98E;(9E)-9-tricosene;(9E)-tricos-9-ene;9-Tricosene,(9E)-;MUSCALURE, (E)-;DTXSID6035734;LMFA11000566;AKOS015899572;3-[1,2,4]Triazol-1-ylmethyl-benzoicacid;LS-157047;Q27289534

Chemical Property of 9-Tricosene

Chemical Property:

• Boiling Point: 399.4 °C at 760 mmHg
• Flash Point: 208.9 °C
• PSA: 0.00000
• Density: 0.802 g/cm³
• LogP: 8.99430
• XLogP3: 11.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 19
• Exact Mass: 322.359951467
• Heavy Atom Count: 23
• Complexity: 216

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCCC=CCCCCCCCC
• Isomeric SMILES: CCCCCCCCCCCCC/C=C/CCCCCCCC

Technology Process of 9-Tricosene

There total 31 articles about 9-Tricosene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-Diphenylphosphinoyltricosan-10-ol → (Z)-tricos-9-ene (27519-02-4) + trans-9-tricosene (35857-62-6)

Guidance literature:

With potassium hydride; In N,N-dimethyl-formamide; at 50 ℃; for 0.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1002/chem.19970031209

Reference yield:

1-decyne (764-93-2) → trans-9-tricosene (35857-62-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 1) BuLi / 1) THF, HMPA, 2) THF, HMPA

2: H₂, quinoline / Pd/BaSO₄ / light petroleum / Ambient temperature

3: 0.28 g / selenium / 18 h / 170 °C

With quinoline; selenium; n-butyllithium; hydrogen; Pd-BaSO₄; In Petroleum ether;

DOI:10.1080/00397919808006830

Reference yield:

1-bromotridecane (765-09-3) → trans-9-tricosene (35857-62-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 1) BuLi / 1) THF, HMPA, 2) THF, HMPA

2: H₂, quinoline / Pd/BaSO₄ / light petroleum / Ambient temperature

3: 0.28 g / selenium / 18 h / 170 °C

With quinoline; selenium; n-butyllithium; hydrogen; Pd-BaSO₄; In Petroleum ether;

DOI:10.1080/00397919808006830

upstream raw materials:

nonan-1-al

triphenylphosphoniotetradecylid

1-Decene

1-pentadecene