dibutan-2-yl(oxo)stannane

Base Information

• Chemical Name: dibutan-2-yl(oxo)stannane
• CAS No.: 30547-28-5
• Molecular Formula: C₈H₁₈OSn
• Molecular Weight: 248.94
• Mol file: 30547-28-5.mol

Synonyms:

Chemical Property of dibutan-2-yl(oxo)stannane

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of dibutan-2-yl(oxo)stannane

There total 1 articles about dibutan-2-yl(oxo)stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(sec-C4H9)2SnBr2 (30547-22-9) → di-s-butyltin oxide (30547-28-5)

Guidance literature:

With sodium hydroxide; In water; react. of tin-compd. with 2 equiv. NaOH (0.1 N);

DOI:10.1016/0022-328X(92)83381-Q

Reference yield: 70.0%

di-s-butyltin oxide (30547-28-5) + 2-Methoxybenzoic acid (579-75-9) → {di-s-butyltin(IV) (2-methoxybenzoate)2} (149439-06-5)

Guidance literature:

In benzene; byproducts: H2O; to a benzene suspension of s-Bu2SnO is added a soln. of 2-methoxybenzoic acid, mixt. is refluxed for 3 h; water (formed during the react.) is removed azeotropically, clear soln. is stripped off in vac., residue is recrystd. from hot acetone, elem. anal.;

Reference yield:

di-s-butyltin oxide (30547-28-5) → {di-s-butyltin(IV) (benzoate)2} (149439-08-7)

Guidance literature:

With benzoic acid; In benzene; byproducts: H2O; to a benzene suspension of s-Bu2SnO is added a soln. of benzoic acid, mixt. is refluxed for 3 h; water (formed during the react.) is removed azeotropically, clear soln. is stripped off in vac., residue is recrystd. from hot acetone, elem. anal.;

upstream raw materials:

(sec-C₄H₉)2SnBr₂

Downstream raw materials:

{di-s-butyltin(IV) (2-methoxybenzoate)2}

{di-s-butyltin(IV) (benzoate)2}

Refernces