thiolane 1,1-dioxide

Base Information

• Chemical Name: thiolane 1,1-dioxide
• CAS No.: 208252-54-4
• Molecular Formula: C₄H₈O₂S
• Molecular Weight: 120.172
• Mol file: 208252-54-4.mol

Synonyms:Thiolane-1,1-dioxide;thiolane1,1-dioxide

Chemical Property of thiolane 1,1-dioxide

Chemical Property:

• Melting Point: 27.4-27.8oC
• Boiling Point: 285oC
• PSA: 42.52000
• LogP: 1.27580

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of thiolane 1,1-dioxide

There total 13 articles about thiolane 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

thiophene (110-01-0) → sulfolane (126-33-0,208252-54-4)

Guidance literature:

With silica gel; magnesium monoperoxyphthalate hexahydrate; In dichloromethane; for 0.833333h; Heating;

DOI:10.1080/00397919808004877

Reference yield: 100.0%

3-Sulfolene (77-79-2) → sulfolane (126-33-0,208252-54-4)

Guidance literature:

With triethylsilane; 1% Pd on activated carbon; In water; at 45 ℃; for 20h; chemoselective reaction; Green chemistry;

DOI:10.1039/d0gc02087g

Reference yield: 87.0%

thiophene (110-01-0) → 1-oxothiolane (1600-44-8) + sulfolane (126-33-0,208252-54-4)

Guidance literature:

With urea-hydrogen peroxide; at 85 ℃; for 0.116667h;

DOI:10.1021/ol990522n

upstream raw materials:

thiophene

3-Sulfolene

3-Isopropoxythiolane 1,3-dioxide

1-oxothiolane

Downstream raw materials:

C₁₈H₁₈

1,2-dimethyl-cyclobutene

1-methanesulfonyl-butane

5-chlorosulfonylisatin