1,2-BenzenediaMine, 3,4-difluoro-N2-(2-fluoro-4-iodophenyl)-6-Methoxy-

Base Information

Chemical Name:1,2-BenzenediaMine, 3,4-difluoro-N2-(2-fluoro-4-iodophenyl)-6-Methoxy-
CAS No.:923032-74-0
Molecular Formula:C13H10F3IN2O
Molecular Weight:394.135
Hs Code.:

Synonyms:1,2-BenzenediaMine, 3,4-difluoro-N2-(2-fluoro-4-iodophenyl)-6-Methoxy-

Suppliers and Price of 1,2-BenzenediaMine, 3,4-difluoro-N2-(2-fluoro-4-iodophenyl)-6-Methoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5,6-DIFLUORO-N1-(2-FLUORO-4-IODOPHENYL)-3-METHOXYBENZENE-1,2-DIAMINE 95.00%
5MG
$ 496.73

Total 1 raw suppliers

Chemical Property of 1,2-BenzenediaMine, 3,4-difluoro-N2-(2-fluoro-4-iodophenyl)-6-Methoxy-

Chemical Property:

PSA：47.28000
LogP:4.69710

Purity/Quality:

99% ^*data from raw suppliers

5,6-DIFLUORO-N1-(2-FLUORO-4-IODOPHENYL)-3-METHOXYBENZENE-1,2-DIAMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2-BenzenediaMine, 3,4-difluoro-N2-(2-fluoro-4-iodophenyl)-6-Methoxy-

There total 5 articles about 1,2-BenzenediaMine, 3,4-difluoro-N2-(2-fluoro-4-iodophenyl)-6-Methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.3%

: 923032-72-8
(2,3-difluoro-5-methoxy-6-nitro-phenyl)-(2-fluoro-4-iodo-phenyl)-amine

: 923032-74-0
3,4-difluoro-N₂-(2-fluoro-4-iodo-phenyl)-6-methoxy-benzene-1,2-diamine

Guidance literature:: With iron; ammonium chloride; In ethanol; for 16h; Heating / reflux;

Reference yield:

: 923032-72-8
(2,3-difluoro-5-methoxy-6-nitro-phenyl)-(2-fluoro-4-iodo-phenyl)-amine

: 923032-74-0
3,4-difluoro-N₂-(2-fluoro-4-iodo-phenyl)-6-methoxy-benzene-1,2-diamine

: Desiodo-DIM-DAB

Guidance literature:: With hydrogen; In tetrahydrofuran; water; at 60 ℃; Flow reactor; Industrial scale;
DOI:10.1021/acs.oprd.7b00039

Reference yield:

: 29632-74-4
2-fluro-4-iodoaniline

: 923032-74-0
3,4-difluoro-N₂-(2-fluoro-4-iodo-phenyl)-6-methoxy-benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / hexane; tetrahydrofuran / 1 h / -78 °C

1.2: 1 h / 20 °C

2.1: tetrahydrofuran / -78 - 20 °C

3.1: hydrogenchloride / water; tetrahydrofuran / 0.08 h

3.2: 20 °C

With hydrogenchloride; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; water;