2-Pyrimidineacetic acid, 1-ethyl-1,2-dihydro-2-hydroxy-4,6-dimethyl-, ethyl ester

Base Information

• Chemical Name: 2-Pyrimidineacetic acid, 1-ethyl-1,2-dihydro-2-hydroxy-4,6-dimethyl-, ethyl ester
• CAS No.: 947322-84-1
• Molecular Formula: C₁₂H₂₀N₂O₃
• Molecular Weight: 240.302
• Mol file: 947322-84-1.mol

Synonyms:2-Pyrimidineacetic acid, 1-ethyl-1,2-dihydro-2-hydroxy-4,6-dimethyl-, ethyl ester

Chemical Property of 2-Pyrimidineacetic acid, 1-ethyl-1,2-dihydro-2-hydroxy-4,6-dimethyl-, ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-Pyrimidineacetic acid, 1-ethyl-1,2-dihydro-2-hydroxy-4,6-dimethyl-, ethyl ester

There total 1 articles about 2-Pyrimidineacetic acid, 1-ethyl-1,2-dihydro-2-hydroxy-4,6-dimethyl-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2-(ethoxycarbonyl)methyl-1-ethyl-4,6-dimethylpyrimidinium iodide → 2-(ethoxycarbonyl)methyl-1-ethyl-2-hydroxy-4,6-dimethyl-1,2-dihydropyrimidine (947322-84-1)

Guidance literature:

With potassium hydroxide; In ethanol; at 0 ℃;

DOI:10.1007/s10593-006-0161-8

Reference yield: 99.0%

2-(ethoxycarbonyl)methyl-1-ethyl-2-hydroxy-4,6-dimethyl-1,2-dihydropyrimidine (947322-84-1) → 2-(ethoxycarbonyl)methylidene-1-ethyl-4,6-dimethyl-1,2-dihydropyrimidine (947322-86-3)

Guidance literature:

In chloroform; Heating;

DOI:10.1007/s10593-006-0161-8

Downstream raw materials:

2-(ethoxycarbonyl)methylidene-1-ethyl-4,6-dimethyl-1,2-dihydropyrimidine