1-(2-Hydroxyphenyl)-3-(piperidino)-2-propene-1-one

Base Information

• Chemical Name: 1-(2-Hydroxyphenyl)-3-(piperidino)-2-propene-1-one
• CAS No.: 1084-62-4
• Molecular Formula: C₁₄H₁₇NO₂
• Molecular Weight: 231.294
• Hs Code.: 2933399090
• Mol file: 1084-62-4.mol

Synonyms:1-(2-Hydroxyphenyl)-3-(piperidino)-2-propene-1-one;1-(2-Hydroxyphenyl)-3-piperidino-2-propen-1-one;2'-Hydroxy-β-piperidinoacrylophenone;(E)-1-(2-hydroxyphenyl)-3-(piperidin-1-yl)prop-2-en-1-one

Chemical Property of 1-(2-Hydroxyphenyl)-3-(piperidino)-2-propene-1-one

Chemical Property:

• PSA: 40.54000
• LogP: 2.51240

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• General Description: 1-(2-Hydroxyphenyl)-3-(piperidino)-2-propene-1-one is a compound synthesized through the reaction of 3-formyl chromones with piperidine under ultrasonic irradiation, demonstrating an efficient method for its preparation. This approach highlights the utility of sonochemistry in facilitating the formation of such enaminone derivatives, which are of interest in organic synthesis and potential pharmacological applications. 1-(2-Hydroxyphenyl)-3-(piperidino)-2-propene-1-one features a hydroxyphenyl group conjugated with a piperidino-substituted propenone moiety, contributing to its structural and electronic properties.

Technology Process of 1-(2-Hydroxyphenyl)-3-(piperidino)-2-propene-1-one

There total 9 articles about 1-(2-Hydroxyphenyl)-3-(piperidino)-2-propene-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

piperidine (110-89-4) + 3-Formylchromone (17422-74-1) → 1-(2-hydroxy-phenyl)-3-piperidin-1-yl-propenone (1084-62-4)

Guidance literature:

In ethanol; for 0.416667h; sonication;

DOI:10.1080/00397910500385266

Reference yield: 63.0%

piperidine (110-89-4) + 3-iodo-chromen-4-one (122775-34-2) → 1-(2-hydroxy-phenyl)-3-piperidin-1-yl-propenone (1084-62-4) + 3-iodo-2-piperidino-4H-1-benzopyran-4-one

Guidance literature:

With potassium carbonate; In acetonitrile;

DOI:10.3987/COM-01-9169

Reference yield: 24.0%

piperidine (110-89-4) + 3-bromo-4H-chromen-4-one (49619-82-1) → 1-(2-hydroxy-phenyl)-3-piperidin-1-yl-propenone (1084-62-4) + 3-(1-piperidinyl)-4H-1-benzopyran-4-one (40302-79-2) + 3-iodo-2-piperidino-4H-1-benzopyran-4-one

Guidance literature:

With iodine; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

DOI:10.3987/COM-01-9169

upstream raw materials:

piperidine

1-benzopyran-4(4H)-one

3-bromo-4H-chromen-4-one

3-iodo-chromen-4-one

Downstream raw materials:

3-amino-4H-chromen-4-one

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