1H-Cyclopentcisoxazole-4,5,6-triol, hexahydro-1-methyl-3-(phenylthio)-, 3R-(3.alpha.,3a.beta.,4.beta.,5.alpha.,6.beta.,6a.beta.)-

Base Information

Chemical Name:1H-Cyclopentcisoxazole-4,5,6-triol, hexahydro-1-methyl-3-(phenylthio)-, 3R-(3.alpha.,3a.beta.,4.beta.,5.alpha.,6.beta.,6a.beta.)-
CAS No.:88111-90-4
Molecular Formula:C13H17NO4S
Molecular Weight:283.34
Hs Code.:
Mol file:88111-90-4.mol

Synonyms:1H-Cyclopentcisoxazole-4,5,6-triol, hexahydro-1-methyl-3-(phenylthio)-, 3R-(3.alpha.,3a.beta.,4.beta.,5.alpha.,6.beta.,6a.beta.)-

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Cyclopentcisoxazole-4,5,6-triol, hexahydro-1-methyl-3-(phenylthio)-, 3R-(3.alpha.,3a.beta.,4.beta.,5.alpha.,6.beta.,6a.beta.)-

Chemical Property:

PSA：98.46000
LogP:0.00080

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Cyclopentcisoxazole-4,5,6-triol, hexahydro-1-methyl-3-(phenylthio)-, 3R-(3.alpha.,3a.beta.,4.beta.,5.alpha.,6.beta.,6a.beta.)-

There total 2 articles about 1H-Cyclopentcisoxazole-4,5,6-triol, hexahydro-1-methyl-3-(phenylthio)-, 3R-(3.alpha.,3a.beta.,4.beta.,5.alpha.,6.beta.,6a.beta.)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 88111-83-5
(1R,5S)-6-exo,7-endo,8-exo-triacetoxy-N-methyl-4-endo-phenylthio-3-oxa-2-azabicyclo<3.3.0>octane

: 88111-90-4
(1R,5S)-6-exo,7-endo,8-exo-trihydroxy-N-methyl-4-endo-phenylthio-3-oxa-2-azabicyclo<3.3.0>octane

Guidance literature:: With sodium methylate; In methanol;

Reference yield:

: Acetic acid (E)-(1S,2R)-2-acetoxy-1-((R)-1-acetoxy-2-oxo-ethyl)-4-phenylsulfanyl-but-3-enyl ester

: 88111-90-4
(1R,5S)-6-exo,7-endo,8-exo-trihydroxy-N-methyl-4-endo-phenylthio-3-oxa-2-azabicyclo<3.3.0>octane

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / pyridine, N-methylhydroxylamine hydrochloride / ethanol / 0.5 h / 50 °C

2: 82 percent / sodium methoxide / methanol

With pyridine; N-methylhydroxyamine hydrochloride; sodium methylate; In methanol; ethanol;