7-[[4-[(2,6-dimethylphenyl)amino]benzoyl]methylamino]Heptanoic acid methyl ester

Base Information

Chemical Name:7-[[4-[(2,6-dimethylphenyl)amino]benzoyl]methylamino]Heptanoic acid methyl ester
CAS No.:1316216-11-1
Molecular Formula:C₂₄H₃₂N₂O₃
Molecular Weight:396.53
Hs Code.:

Synonyms:7-[[4-[(2,6-dimethylphenyl)amino]benzoyl]methylamino]Heptanoic acid methyl ester

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Chemical Property of 7-[[4-[(2,6-dimethylphenyl)amino]benzoyl]methylamino]Heptanoic acid methyl ester

Chemical Property:

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Technology Process of 7-[[4-[(2,6-dimethylphenyl)amino]benzoyl]methylamino]Heptanoic acid methyl ester

There total 7 articles about 7-[[4-[(2,6-dimethylphenyl)amino]benzoyl]methylamino]Heptanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1316216-10-0
C₁₆H₂₂BrNO₃

: 87-62-7
2,6-dimethylaniline

: 1316216-11-1
C₂₄H₃₂N₂O₃

Guidance literature:: With caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 100 ℃;

Reference yield:

: 17994-94-4
methyl 7-aminoheptanoate hydrochloride

: 1316216-11-1
C₂₄H₃₂N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 4 h / 20 °C

1.2: 20 °C

2.1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 10.03 h / 0 °C / Reflux

2.2: 1 h / Reflux

3.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 4 h / 20 °C

4.1: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 100 °C

With carbonochloridic acid 1-chloro-ethyl ester; sodium tris(acetoxy)borohydride; caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In dichloromethane; 1,2-dichloro-ethane; toluene;

Reference yield:

: 929-17-9
7-aminoheptanoic acid

: 1316216-11-1
C₂₄H₃₂N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / -10 - 20 °C

2.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 4 h / 20 °C

2.2: 20 °C

3.1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 10.03 h / 0 °C / Reflux

3.2: 1 h / Reflux

4.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 4 h / 20 °C

5.1: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 100 °C

With thionyl chloride; carbonochloridic acid 1-chloro-ethyl ester; sodium tris(acetoxy)borohydride; caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In dichloromethane; 1,2-dichloro-ethane; toluene;