Dibutyl 4-butoxy-2,6-pyridinedicarboxylate

Base Information

Chemical Name:Dibutyl 4-butoxy-2,6-pyridinedicarboxylate
CAS No.:173314-94-8
Molecular Formula:C₁₉H₂₉NO₅
Molecular Weight:351.443
Hs Code.:
Mol file:173314-94-8.mol

Synonyms:Dibutyl 4-butoxy-2,6-pyridinedicarboxylate

Suppliers and Price of Dibutyl 4-butoxy-2,6-pyridinedicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
DIBUTYL-4-BUTOXY-2,6-PYRIDINEDICARBOXYLATE 95.00%
5MG
$ 497.37

Total 1 raw suppliers

Chemical Property of Dibutyl 4-butoxy-2,6-pyridinedicarboxylate

Chemical Property:

Vapor Pressure:4.62E-09mmHg at 25°C
Boiling Point:471.5°C at 760 mmHg
Flash Point:239°C
PSA：74.72000
Density:1.061g/cm³
LogP:4.17430

Purity/Quality:: DIBUTYL-4-BUTOXY-2,6-PYRIDINEDICARBOXYLATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Dibutyl 4-butoxy-2,6-pyridinedicarboxylate

There total 2 articles about Dibutyl 4-butoxy-2,6-pyridinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 499-51-4
Chelidamic acid

: 71-36-3
butan-1-ol

: 173314-94-8
dibutyl 4-butoxypyridine-2,6-dicarboxylate

Guidance literature:: With sulfuric acid; for 24h; Heating;
DOI:10.1021/ja00155a006

Reference yield: 14.0%

: 542-69-8
1-iodo-butane

: 499-51-4
Chelidamic acid

: 173314-94-8
dibutyl 4-butoxypyridine-2,6-dicarboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.03.024

Reference yield:

: 173314-94-8
dibutyl 4-butoxypyridine-2,6-dicarboxylate

: 852998-13-1
(2,6-diamino-4-butoxy-pyridin-3-yl)-(2,6-difluoro-phenyl)-methanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: N₂H₂ / ethanol

2.1: NaNO₂; HCl / 1 h / 0 °C

3.1: Heating

4.1: n-BuLi; (N,N,N',N'-tetramethyl)ethylenediamine / various solvent(s) / 16 h / -15 - 0 °C

4.2: 37 percent / various solvent(s) / 3 h / 0 °C

5.1: 86 percent / TFA / CH₂Cl₂ / 5 h / 20 °C

With hydrogenchloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diazene; trifluoroacetic acid; sodium nitrite; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2005.03.024