2-Methyl-5-(tributylstannyl)pyridine

Base Information

Chemical Name:2-Methyl-5-(tributylstannyl)pyridine
CAS No.:167556-64-1
Molecular Formula:C18H33NSn
Molecular Weight:382.177
Hs Code.:
DSSTox Substance ID:DTXSID40592853
Wikidata:Q82487186
Mol file:167556-64-1.mol

Synonyms:2-Methyl-5-(tributylstannyl)pyridine;167556-64-1;tributyl-(6-methylpyridin-3-yl)stannane;Pyridine, 2-methyl-5-(tributylstannyl)-;MFCD12827559;SCHEMBL1456734;DTXSID40592853;GQSHSSUYFVJPOO-UHFFFAOYSA-N;2-methyl-5-tributylstannanyl-pyridine;AKOS015843076;SY319005;DB-217479;EN300-193021;2-Methyl-5-(tributylstannyl)pyridine, AldrichCPR;A909910;J-509992

Suppliers and Price of 2-Methyl-5-(tributylstannyl)pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
2-Methyl-5-(tributylstannyl)pyridine Aldrich
1g
$ 258.00

Matrix Scientific
2-Methyl-5-(tributylstannyl)pyridine 96%
1g
$ 322.00

Matrix Scientific
2-Methyl-5-(tributylstannyl)pyridine 96%
500mg
$ 208.00

Matrix Scientific
2-Methyl-5-(tributylstannyl)pyridine 96%
5g
$ 1042.00

Alichem
2-Methyl-5-(tributylstannyl)pyridine
5g
$ 821.94

AK Scientific
2-Methyl-5-(tributylstannyl)pyridine
5g
$ 691.00

Total 12 raw suppliers

Chemical Property of 2-Methyl-5-(tributylstannyl)pyridine

Chemical Property:

Vapor Pressure:8.51E-06mmHg at 25°C
Boiling Point:385.3°C at 760 mmHg
PKA:5.93±0.12(Predicted)
Flash Point:186.8°C
PSA：12.89000
LogP:5.44610
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:10
Exact Mass:383.163503
Heavy Atom Count:20
Complexity:220

Purity/Quality:

97% ^*data from raw suppliers

2-Methyl-5-(tributylstannyl)pyridine Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC[Sn](CCCC)(CCCC)C1=CN=C(C=C1)C

Technology Process of 2-Methyl-5-(tributylstannyl)pyridine

There total 1 articles about 2-Methyl-5-(tributylstannyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3430-13-5
5-bromo-2-methylpyridine

: 1461-22-9
tributyltin chloride

: 167556-64-1
2-methyl-5-(tributylstannyl)pyridine

Guidance literature:: 5-bromo-2-methylpyridine; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 1h;

tributyltin chloride; In diethyl ether; hexane; at -78 - 0 ℃; for 1h;

With water; ammonium chloride; In diethyl ether; hexane;

Reference yield: 84.0%

: benzyl (4S,5S)-5-{(2S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropyl}-2,2-dimethyl-4-{4-[(trifluoroacetyl)oxy]benzyl}-1,3-oxazolidine-3-carboxylate

: 167556-64-1
2-methyl-5-(tributylstannyl)pyridine

: 854756-82-4
benzyl (4S,5S)-5-{(2S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropyl}-2,2-dimethyl-4-[4-(6-methyl-3-pyridinyl)benzyl]-1,3-oxazolidine-3-carboxylate

Guidance literature:: benzyl (4S,5S)-5-{(2S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropyl}-2,2-dimethyl-4-{4-[(trifluoroacetyl)oxy]benzyl}-1,3-oxazolidine-3-carboxylate; 2-methyl-5-(tributylstannyl)pyridine; With lithium chloride; bis-triphenylphosphine-palladium(II) chloride; In DMF (N,N-dimethyl-formamide); at 100 ℃; for 16h;

With water; In DMF (N,N-dimethyl-formamide); ethyl acetate;