LinearBtrisaccharide

Base Information

• Chemical Name: LinearBtrisaccharide
• CAS No.: 101627-01-4
• Molecular Formula: C₂₀H₃₅NO₁₆
• Molecular Weight: 545.495
• Mol file: 101627-01-4.mol

Synonyms:O-alpha-D-Galactopyranosyl-(1-3)-O-beta-D-galactopyranosyl-(1-4)-2-(acetylamino)-2-deoxy-beta-D-glucopyranose

Chemical Property of LinearBtrisaccharide

Chemical Property:

• Boiling Point: 998.1±65.0 °C(Predicted)
• PKA: 11.93±0.70(Predicted)
• PSA: 277.55000
• Density: 1.71±0.1 g/cm3(Predicted)
• LogP: -7.03830

Purity/Quality:

95% ^*data from raw suppliers

LINEAR B-2 TRISACCHARIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of LinearBtrisaccharide

There total 18 articles about LinearBtrisaccharide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

benzyl 2-acetamido-4-O-<2,6-di-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside (77356-44-6) → Galα(1->3)Galβ(1->4)GlcNAc (59446-75-2,72398-11-9,92762-38-4,101627-01-4,146863-51-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid; for 24h;

DOI:10.1039/P19810000326

Reference yield: 56.0%

UDP-glucose (133-89-1) + N-acetyl-D-lactosamine (4307-58-8,6050-69-7,30868-22-5,34641-68-4,36954-65-1,47491-70-3,58718-18-6,60966-24-7,62929-48-0,69610-06-6,71698-59-4,75917-82-7,87982-93-2,87982-94-3,93601-71-9,109121-51-9,135760-02-0) → Galα(1->3)Galβ(1->4)GlcNAc (59446-75-2,72398-11-9,92762-38-4,101627-01-4,146863-51-6)

Guidance literature:

With Tris-HCl buffer; α(1->3)-galactosyltransferase; UDP-galactose-4-epimerase; manganese(ll) chloride; bovine serum albumin; at 25 ℃; for 72h;

DOI:10.1021/ja9808898

Reference yield: 48.0%

N-acetyl-D-lactosamine (4307-58-8,6050-69-7,30868-22-5,34641-68-4,36954-65-1,47491-70-3,58718-18-6,60966-24-7,62929-48-0,69610-06-6,71698-59-4,75917-82-7,87982-93-2,87982-94-3,93601-71-9,109121-51-9,135760-02-0) + 4-nitrophenyl α-D-galactoside (7493-95-0) → Galα(1->3)Galβ(1->4)GlcNAc (59446-75-2,72398-11-9,92762-38-4,101627-01-4,146863-51-6)

Guidance literature:

With citrate-phosphate buffer; α-galactosidase from Penicillium multicolor; at 30 ℃; for 6h; pH=4.0;

DOI:10.1039/a906020k

upstream raw materials:

O-(2-O-Acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1-> 3)-O-(6-O-acetyl-2,4-di-O-benzyl-β-D-mannopyranosyl)-(1-> 4)-1,6-anhydro-2-azido-3-O-benzyl-2-desoxy-β-D-glucopyranose

benzyl 2-acetamido-4-O-<2,6-di-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

O-α-L-fucopyranosyl-(1<*>2)-3)>-O-β-D-galactopyranosyl-(1<*>4)-2-acetamido-2-deoxy-D-glucopyranose

UDP-glucose

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