Bis(2-fluorobenzyl)aMine, 97%

Base Information

• Chemical Name: Bis(2-fluorobenzyl)aMine, 97%
• CAS No.: 823188-83-6
• Molecular Formula: C14H13F2N
• Molecular Weight: 233.261
• Mol file: 823188-83-6.mol

Synonyms:Bis(2-fluorobenzyl)aMine, 97%

Chemical Property of Bis(2-fluorobenzyl)aMine, 97%

Chemical Property:

• Boiling Point: 306.5±27.0 °C(Predicted)
• PKA: 7.37±0.20(Predicted)
• PSA: 12.03000
• Density: 1.165±0.06 g/cm3(Predicted)
• LogP: 3.64550

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bis(2-fluorobenzyl)aMine, 97%

There total 4 articles about Bis(2-fluorobenzyl)aMine, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2-fluorobenzonitrile (394-47-8) → N,N-bis[(2-fluorophenyl)methyl]amine (823188-83-6)

Guidance literature:

With borane-ammonia complex; (9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene)dichlorocobalt(II); at 27 ℃; for 16h; Glovebox; Inert atmosphere;

DOI:10.1002/adsc.201900586

Reference yield:

2-Fluorobenzaldehyde (446-52-6) → N,N-bis[(2-fluorophenyl)methyl]amine (823188-83-6)

Guidance literature:

With ammonia; hydrogen; In methanol; at 90 ℃; for 15h; under 15001.5 Torr; Autoclave;

DOI:10.1002/cctc.202101587

Reference yield:

2-fluorobenzylamine (89-99-6) → N,N-bis[(2-fluorophenyl)methyl]amine (823188-83-6)

Guidance literature:

With oxygen; at 24.84 ℃; for 8h; under 760.051 Torr; Irradiation;

DOI:10.1007/s11426-021-1066-7

upstream raw materials:

2-fluorobenzonitrile

2-fluorobenzylamine

2-Fluorobenzaldehyde