5-phenyl-5,12- dihydroindolo [3,2-a]carbazole

Base Information

• Chemical Name: 5-phenyl-5,12- dihydroindolo [3,2-a]carbazole
• CAS No.: 1247053-55-9
• Molecular Formula: C24H16N2
• Molecular Weight: 332.404
• Mol file: 1247053-55-9.mol

Synonyms:5-phenyl-5,12- dihydroindolo [3,2-a]carbazole;5,12-Dihydro-5-phenylindolo[3,2-a]carbazole

Chemical Property of 5-phenyl-5,12- dihydroindolo [3,2-a]carbazole

Chemical Property:

• Melting Point: 170 °C
• Boiling Point: 598.8±32.0 °C(Predicted)
• PKA: 16.87±0.30(Predicted)
• PSA: 20.72000
• Density: 1.26±0.1 g/cm3(Predicted)
• LogP: 6.41820
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

99.0% ^*data from raw suppliers

5-Phenyl-5,12-dihydroindolo[3,2-a]carbazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-phenyl-5,12- dihydroindolo [3,2-a]carbazole

There total 20 articles about 5-phenyl-5,12- dihydroindolo [3,2-a]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

iodobenzene (591-50-4) + 7,12-dihydropyrido<3,2-b;5,4-b'>diindole (111296-91-4) → 5,12-dihydro-5-phenyl indolo[3,2-a]carbazole (1247053-55-9)

Guidance literature:

With potassium phosphate; copper(l) iodide; rac-diaminocyclohexane; In m-xylene; at 155 ℃;

Reference yield: 89.0%

3-(2-nitrophenyl)-9-phenyl-9H-carbazole (1260032-04-9) → 5,12-dihydro-5-phenyl indolo[3,2-a]carbazole (1247053-55-9)

Guidance literature:

With triethyl phosphite; In 1,2-dichloro-benzene; at 180 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.dyepig.2018.10.060

Reference yield: 65.0%

bromobenzene (108-86-1,52753-63-6) + 7,12-dihydropyrido<3,2-b;5,4-b'>diindole (111296-91-4) → 5,12-dihydro-5-phenyl indolo[3,2-a]carbazole (1247053-55-9)

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; potassium hydroxide; In dimethyl sulfoxide; for 15h; Inert atmosphere; Reflux;

upstream raw materials:

indole

iodobenzene

7,12-dihydropyrido<3,2-b;5,4-b'>diindole

2,3-dihydro-1H,1'H-[2,3']biindolyl

Downstream raw materials:

C₃₅H₂₃N₃

C₄₁H₂₆N₄

C₄₄H₂₆N₄O

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