(S)-b-AMino-3-Methoxy-benzeneethanol

Base Information

• Chemical Name: (S)-b-AMino-3-Methoxy-benzeneethanol
• CAS No.: 1213016-49-9
• Molecular Formula: C9H13NO2
• Molecular Weight: 167.20502
• Hs Code.: 2922500090
• Mol file: 1213016-49-9.mol

Synonyms:(S)-b-AMino-3-Methoxy-benzeneethanol;(2S)-2-AMINO-2-(3-METHOXYPHENYL)ETHAN-1-OL;(S)-2-Amino-2-(3-methoxyphenyl)ethanol;(2S)-2-amino-2-(3-methoxyphenyl)ethanol

Chemical Property of (S)-b-AMino-3-Methoxy-benzeneethanol

Chemical Property:

• PSA: 55.48000
• LogP: 1.38760
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

99% ^*data from raw suppliers

(S)-2-Amino-2-(3-methoxyphenyl)ethanol 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-b-AMino-3-Methoxy-benzeneethanol

There total 14 articles about (S)-b-AMino-3-Methoxy-benzeneethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

(R)-2-azido-2-(3-methoxyphenyl)ethan-1-ol → (R)-2-amino-2-(3-methoxyphenyl)ethanol (1213016-49-9,763080-04-2)

Guidance literature:

With water; triphenylphosphine; In tetrahydrofuran; at 70 ℃;

DOI:10.1016/j.tetasy.2015.12.002

Reference yield: 80.0%

(Rs,1S)-N-(2-(tert-butyldimethylsilyloxy)-1-(3-methoxyphenyl)ethyl)-2-methylpropane-2-sulfinamide (1312719-13-3) → (S)-2-amino-2-(3-methoxyphenyl)ethanol (1213016-49-9,763080-04-2)

Guidance literature:

(Rs,1S)-N-(2-(tert-butyldimethylsilyloxy)-1-(3-methoxyphenyl)ethyl)-2-methylpropane-2-sulfinamide; With hydrogenchloride; In methanol; at 20 ℃; for 3h;

With sodium hydrogencarbonate; In water;

DOI:10.1016/j.tetasy.2011.01.011

Reference yield:

C9H11NO3 → 2-amino-2-(3-methoxyphenyl)ethan-1-ol (325153-00-2,1213016-49-9,763080-04-2)

Guidance literature:

With hydrogen; nickel;

DOI:10.1021/jo9011255

upstream raw materials:

(Rs)-N-(2-(tert-butyldimethylsilyloxy)-1-(3-methoxyphenyl)ethylidene)-2-methylpropane-2-sulfinamide

(Rs,1S)-N-(2-(tert-butyldimethylsilyloxy)-1-(3-methoxyphenyl)ethyl)-2-methylpropane-2-sulfinamide

2-(tert-butyldimethylsilyloxy)-1-(3-methoxyphenyl)ethanone

3-methoxyphenyl bromide