Tert-butyl 2-(2,2-diMethyl-4h-benzo[d][1,3]dioxin-6-yl)-2-hydroxyethylcarbaMate

Base Information

Chemical Name:Tert-butyl 2-(2,2-diMethyl-4h-benzo[d][1,3]dioxin-6-yl)-2-hydroxyethylcarbaMate
CAS No.:452340-95-3
Molecular Formula:C17H25NO5
Molecular Weight:323.3841
Hs Code.:
Mol file:452340-95-3.mol

Synonyms:Tert-butyl 2-(2,2-diMethyl-4h-benzo[d][1,3]dioxin-6-yl)-2-hydroxyethylcarbaMate

Suppliers and Price of Tert-butyl 2-(2,2-diMethyl-4h-benzo[d][1,3]dioxin-6-yl)-2-hydroxyethylcarbaMate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 5 raw suppliers

Chemical Property of Tert-butyl 2-(2,2-diMethyl-4h-benzo[d][1,3]dioxin-6-yl)-2-hydroxyethylcarbaMate

Chemical Property:

Boiling Point:488.6±45.0 °C(Predicted)
PKA:12.17±0.46(Predicted)
PSA：77.02000
Density:1.143±0.06 g/cm3(Predicted)
LogP:3.28070

Purity/Quality:: NLT 98% ^*data from raw suppliers

Safty Information:

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Technology Process of Tert-butyl 2-(2,2-diMethyl-4h-benzo[d][1,3]dioxin-6-yl)-2-hydroxyethylcarbaMate

There total 2 articles about Tert-butyl 2-(2,2-diMethyl-4h-benzo[d][1,3]dioxin-6-yl)-2-hydroxyethylcarbaMate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 915132-89-7
2-amino-1-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)ethanol

: 24424-99-5
di-tert-butyl dicarbonate

: 452340-95-3
tert-Butyl 2-(2,2-dimethyl-4H-benzo[d][1,3]dioxin-6-yl)-2-hydroxyethylcarbamate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;

Reference yield: 43.0%

: 52113-69-6
6-bromo-2,2-dimethyl-4H-benzo[1,3]dioxine

: 89711-08-0
N-(t-butoxycarbonyl)glycinal

: 452340-95-3
tert-Butyl 2-(2,2-dimethyl-4H-benzo[d][1,3]dioxin-6-yl)-2-hydroxyethylcarbamate

Guidance literature:: 6-bromo-2,2-dimethyl-4H-benzo[1,3]dioxine; With n-butyllithium; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

N-(t-butoxycarbonyl)glycinal; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;