Chloro[(1,2,5,6-η)-1,5-cyclooctadiene](2,2-dimethylpropyl)-palladium 95%

Base Information

Chemical Name:Chloro[(1,2,5,6-η)-1,5-cyclooctadiene](2,2-dimethylpropyl)-palladium 95%
CAS No.:935838-06-5
Molecular Formula:C13H23ClPd
Molecular Weight:321.199
Hs Code.:
Mol file:935838-06-5.mol

Synonyms:Chloro[(1,2,5,6-η)-1,5-cyclooctadiene](2,2-dimethylpropyl)-palladium 95%;Chloro[(1,2,5,6-η)-1,5-cyclooctadiene](2,2-diMethylpropyl)-palladiuM,95%

Suppliers and Price of Chloro[(1,2,5,6-η)-1,5-cyclooctadiene](2,2-dimethylpropyl)-palladium 95%

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
Chloro[(1,2,5,6-η)-1,5-cyclooctadiene](2,2-dimethylpropyl)-palladium 95%
250mg
$ 57.80

American Custom Chemicals Corporation
CHLORO[(1,2,5,6-ETA)-1,5-CYCLOOCTADIENE](2,2-DIMETHYLPROPYL)-PALLADIUM 95.00%
250MG
$ 602.25

Total 4 raw suppliers

Chemical Property of Chloro[(1,2,5,6-η)-1,5-cyclooctadiene](2,2-dimethylpropyl)-palladium 95%

Chemical Property:

Melting Point:105-110°C
PSA：0.00000
LogP:1.54340

Purity/Quality:

99% ^*data from raw suppliers

Chloro[(1,2,5,6-η)-1,5-cyclooctadiene](2,2-dimethylpropyl)-palladium 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Chloro[(1,2,5,6-η)-1,5-cyclooctadiene](2,2-dimethylpropyl)-palladium 95%

There total 1 articles about Chloro[(1,2,5,6-η)-1,5-cyclooctadiene](2,2-dimethylpropyl)-palladium 95% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 7412-67-1
neopentyl lithium

: 935838-06-5
[PdCl(neopentyl)(1,5-COD)]

Guidance literature:: In diethyl ether; (inert atm.); addn. of ethereal soln. of neopentyllithium to ethereal suspn. of palladium compd. at -75°C for 1.5 h, stirring at -75°C for 1 h, warming to room temp., stirring for 3 h; filtration through celite, evapn., recrystn. (pentane) at -20°C, elem. anal.;
DOI:10.1021/om800455h

Reference yield: 80.0%

: 935838-06-5
[PdCl(neopentyl)(1,5-COD)]

: 244187-81-3
1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene

: cis-[Pd₂Cl₂(neopentyl)2(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene)2]

Guidance literature:: In tetrahydrofuran; (inert atm.); addn. of THF soln. of 1 equiv. of imidazolylidene deriv. to THF soln. of palladium compd. at 0°C, stirring at 0°C for 30 min, stirring at room temp.; evapn., addn. of pentane, decantation, washing with cold pentane, dryingin vac., elem. anal.;
DOI:10.1021/om800455h