12-Azidododecylphosphonic acid, 95%

Base Information

• Chemical Name: 12-Azidododecylphosphonic acid, 95%
• CAS No.: 721457-32-5
• Molecular Formula: C₁₂H₂₆N₃O₃P
• Molecular Weight: 291.331
• Mol file: 721457-32-5.mol

Synonyms:12-Azidododecylphosphonic acid, 95%

Chemical Property of 12-Azidododecylphosphonic acid, 95%

Chemical Property:

• Melting Point: 83-85℃
• PSA: 117.09000
• LogP: 3.82816
• Storage Temp.: 2-8°C

Purity/Quality:

≥95% ^*data from raw suppliers

12-Azidododecylphosphonic acid, 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 12-Azidododecylphosphonic acid, 95%

There total 2 articles about 12-Azidododecylphosphonic acid, 95% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

diethyl (12-azidododecyl)phosphonate (1242248-75-4) → (12-azidododecyl)phosphonic acid (721457-32-5)

Guidance literature:

diethyl (12-azidododecyl)phosphonate; With trimethylsilyl bromide; In dichloromethane; at 20 ℃; Inert atmosphere;

With water; for 2h; Inert atmosphere;

DOI:10.1021/cm401326p

Reference yield:

1,12-dibromododecane (3344-70-5) → (12-azidododecyl)phosphonic acid (721457-32-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 4 h / 160 °C

2.1: sodium azide / ethanol / 40 h / Reflux

3.1: trimethylsilyl bromide / dichloromethane / 20 °C / Inert atmosphere

3.2: 2 h / Inert atmosphere

With sodium azide; trimethylsilyl bromide; In ethanol; dichloromethane;

DOI:10.1021/cm401326p

upstream raw materials:

diethyl (12-azidododecyl)phosphonate

1,12-dibromododecane