2-De(carboxy)-19-deoxy-2-(methoxycarbonyl)-6β,19-epoxylimonoic acid 16,17-lactone

Base Information

• Chemical Name: 2-De(carboxy)-19-deoxy-2-(methoxycarbonyl)-6β,19-epoxylimonoic acid 16,17-lactone
• CAS No.: 1063-13-4
• Molecular Formula: C27H32O9
• Molecular Weight: 500.53758
• Mol file: 1063-13-4.mol

Synonyms:2-De(carboxy)-19-deoxy-2-(methoxycarbonyl)-6β,19-epoxylimonoic acid 16,17-lactone;Methyl limonilate

Chemical Property of 2-De(carboxy)-19-deoxy-2-(methoxycarbonyl)-6β,19-epoxylimonoic acid 16,17-lactone

Chemical Property:

• Melting Point: 230 - 233 °C
• PSA: 113.80000
• LogP: 2.76230

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-De(carboxy)-19-deoxy-2-(methoxycarbonyl)-6β,19-epoxylimonoic acid 16,17-lactone

There total 3 articles about 2-De(carboxy)-19-deoxy-2-(methoxycarbonyl)-6β,19-epoxylimonoic acid 16,17-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) → (17S)-1α,4;6β,19;14,15β;21,23-tetraepoxy-17-hydroxy-4,4,8-trimethyl-7-oxo-3,4;16,17-diseco-24-nor-5α,13α,14β-chola-20,22-diene-3,16-dioic acid-16-lactone-3-methyl ester (1063-13-4)

Guidance literature:

With 1,4-dioxane; diethyl ether;

DOI:10.1021/ja01123a031

Reference yield:

→ (17S)-1α,4;6β,19;14,15β;21,23-tetraepoxy-17-hydroxy-4,4,8-trimethyl-7-oxo-3,4;16,17-diseco-24-nor-5α,13α,14β-chola-20,22-diene-3,16-dioic acid-16-lactone-3-methyl ester (1063-13-4)

Guidance literature:

With diazomethane; diethyl ether; ethanol;

DOI:10.1021/jo01176a017

Reference yield:

→ Limonilsaeure-methylester (1063-13-4)

Guidance literature:

Limonilsaeure, Diazomethan (Ae.);

upstream raw materials:

diazomethane

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