4,5,6,7-Tetrahydrooxonin

Base Information

• Chemical Name: 4,5,6,7-Tetrahydrooxonin
• CAS No.: 17123-56-7
• Molecular Formula: C8H12O
• Molecular Weight: 124.18
• Mol file: 17123-56-7.mol

Synonyms:4,5,6,7-Tetrahydrooxonin

Chemical Property of 4,5,6,7-Tetrahydrooxonin

Chemical Property:

• PSA: 9.23000
• LogP: 2.60440

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,5,6,7-Tetrahydrooxonin

There total 2 articles about 4,5,6,7-Tetrahydrooxonin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(Z)-3-hydroperoxycyclooct-1-ene (4096-42-8) + Tosyl isocyanate (4083-64-1) → oxacyclonon-2,8-diene (17123-56-7) + C16H21NO5S

Guidance literature:

In chloroform; at 0 ℃;

DOI:10.1021/jo00097a006

Reference yield:

1,3-cyclooctadiene (3806-59-5) → oxacyclonon-2,8-diene (17123-56-7)

Guidance literature:

With diphenylether; Yield given. Multistep reaction; 2.) 255 deg C, 60 min;

upstream raw materials:

1,3-cyclooctadiene

(Z)-3-hydroperoxycyclooct-1-ene

Tosyl isocyanate

Refernces

• 1、 Burt, R. A.,Chiang, Y.,Kresge, A. J.,Szilagyi, S.. "Vinyl ether hydrolysis.XVII. Oxacyclonon-2,8-diene and the question of the unorthodox reaction mechanism for 9-methoxyoxacyclonon-2-ene". . p. 74 - 76. Retrieved 2007/10/02.