6-Deoxy-6-iodo-2-O,3-O,4-O-triacetyl α-D-mannopyranosyl bromide

Base Information

Chemical Name:6-Deoxy-6-iodo-2-O,3-O,4-O-triacetyl α-D-mannopyranosyl bromide
CAS No.:50692-56-3
Molecular Formula:C12H16BrIO7
Molecular Weight:479.06
Hs Code.:
Mol file:50692-56-3.mol

Synonyms:6-Deoxy-6-iodo-2-O,3-O,4-O-triacetyl α-D-mannopyranosyl bromide

Suppliers and Price of 6-Deoxy-6-iodo-2-O,3-O,4-O-triacetyl α-D-mannopyranosyl bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 6-Deoxy-6-iodo-2-O,3-O,4-O-triacetyl α-D-mannopyranosyl bromide

Chemical Property:

Melting Point:136 - 137 °C
PSA：88.13000
LogP:1.33630

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 6-Deoxy-6-iodo-2-O,3-O,4-O-triacetyl α-D-mannopyranosyl bromide

There total 8 articles about 6-Deoxy-6-iodo-2-O,3-O,4-O-triacetyl α-D-mannopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 692776-41-3
1,2,3,4-tetra-O-acetyl-6-O-deoxy-6-iodo-α-D-mannopyranose

: 50692-56-3
2,3,4-tri-O-acetyl-6-deoxy-6-iodo-α-D-mannopyranosyl bromide

Guidance literature:: With hydrogen bromide; acetic acid; at 20 ℃;
DOI:10.1016/j.chemphyslip.2021.105161

Reference yield: 93.4%

: 7468-48-6
6-deoxy-6-iodotetra-O-acetyl-β-D-glucopyranose

: 50692-56-3,95464-10-1
6-Desoxy-6-iod-2,3,4-tri-O-acetyl-α-D-glucopyranosylbromid

Guidance literature:: With hydrogen bromide; acetic acid; In dichloromethane; for 10h;
DOI:10.1016/S0008-6215(00)90732-8

Reference yield:

: 617-04-9
(2R,3S,4S,5S,6S)-2-(hydroxymethyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triol

: 50692-56-3
2,3,4-tri-O-acetyl-6-deoxy-6-iodo-α-D-mannopyranosyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine; triphenylphosphine; 1H-imidazole / tetrahydrofuran / 2 h / Reflux

1.2: 0.5 h / 20 °C

1.3: 20 °C

2.1: hydrogen bromide; acetic acid / 20 °C

With 1H-imidazole; hydrogen bromide; iodine; acetic acid; triphenylphosphine; In tetrahydrofuran;
DOI:10.1016/j.chemphyslip.2021.105161