2-Acetyl-1,2,3,4,4a,5,6,11,12,12a-decahydro-12a-hydroxy-5-(acetoxymethyl)-12-methylpyrido[3',4':5,6]cyclohept[1,2-b]indole-5-carboxylic acid γ-lactone

Base Information

Chemical Name:2-Acetyl-1,2,3,4,4a,5,6,11,12,12a-decahydro-12a-hydroxy-5-(acetoxymethyl)-12-methylpyrido[3',4':5,6]cyclohept[1,2-b]indole-5-carboxylic acid γ-lactone
CAS No.:3368-89-6
Molecular Formula:C23H26N2O5
Molecular Weight:410.46
Hs Code.:
Mol file:3368-89-6.mol

2-Acetyl-1,2,3,4,4a,5,6,11,12,12a-decahydro-12a-hydroxy-5-(acetoxymethyl)-12-methylpyrido[3',4':5,6]cyclohept[1,2-b]indole-5-carboxylic acid γ-lactone

Synonyms:2-Acetyl-1,2,3,4,4a,5,6,11,12,12a-decahydro-12a-hydroxy-5-(acetoxymethyl)-12-methylpyrido[3',4':5,6]cyclohept[1,2-b]indole-5-carboxylic acid γ-lactone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Acetyl-1,2,3,4,4a,5,6,11,12,12a-decahydro-12a-hydroxy-5-(acetoxymethyl)-12-methylpyrido[3',4':5,6]cyclohept[1,2-b]indole-5-carboxylic acid γ-lactone

Chemical Property:

Melting Point:247 - 250 °C (ethyl acetate)
PSA：88.70000
LogP:2.26290

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 2-Acetyl-1,2,3,4,4a,5,6,11,12,12a-decahydro-12a-hydroxy-5-(acetoxymethyl)-12-methylpyrido[3',4':5,6]cyclohept[1,2-b]indole-5-carboxylic acid γ-lactone

There total 4 articles about 2-Acetyl-1,2,3,4,4a,5,6,11,12,12a-decahydro-12a-hydroxy-5-(acetoxymethyl)-12-methylpyrido[3',4':5,6]cyclohept[1,2-b]indole-5-carboxylic acid γ-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3368-87-4,56324-22-2,107657-44-3
(19E)-17-hydroxy-3,7-seco-6-nor-cura-2⁽⁷⁾,19-diene-16-carboxylic acid methyl ester

: 3368-89-6
(5R)-5-acetoxymethyl-2-acetyl-12ξ-methyl-(4ac)-2,3,4,4a,5,6,11,12-octahydro-1H-12ac,5r-oxaethano-pyrido[3',4':5,6]cyclohepta[1,2-b]indol-14-one

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / CH₂Cl₂

2: H₂ / Pd-C / methanol

3: Py

With pyridine; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1002/hlca.19640470750

Reference yield:

: 3329-94-0
(5R)-5-hydroxymethyl-12ξ-methyl-14-oxo-(4ac)-4,4a,5,6,11,12-hexahydro-3H-12ac,5r-oxaethano-pyrido[3',4':5,6]cyclohepta[1,2-b]indole-2-carboxylic acid benzyl ester

: 3368-89-6
(5R)-5-acetoxymethyl-2-acetyl-12ξ-methyl-(4ac)-2,3,4,4a,5,6,11,12-octahydro-1H-12ac,5r-oxaethano-pyrido[3',4':5,6]cyclohepta[1,2-b]indol-14-one

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd-C / methanol

2: Py

With pyridine; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1002/hlca.19640470750