tert-Butyl 4-iodo-2-methylbut-2-enoate

Base Information

Chemical Name:tert-Butyl 4-iodo-2-methylbut-2-enoate
CAS No.:53689-87-5
Molecular Formula:C₉H₁₅IO₂
Molecular Weight:282.121
Hs Code.:2916190090
DSSTox Substance ID:DTXSID70700560
Mol file:53689-87-5.mol

Synonyms:tert-Butyl 4-iodo-2-methylbut-2-enoate;53689-87-5;DTXSID70700560

Suppliers and Price of tert-Butyl 4-iodo-2-methylbut-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
T-BUTYL (E)-4-IODO-2-METHYL-2-BUTENOATE 95.00%
5MG
$ 498.07

Total 0 raw suppliers

Chemical Property of tert-Butyl 4-iodo-2-methylbut-2-enoate

Chemical Property:

PSA：26.30000
LogP:2.70940
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:282.01168
Heavy Atom Count:12
Complexity:189

Purity/Quality:: T-BUTYL (E)-4-IODO-2-METHYL-2-BUTENOATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CCI)C(=O)OC(C)(C)C

Technology Process of tert-Butyl 4-iodo-2-methylbut-2-enoate

There total 4 articles about tert-Butyl 4-iodo-2-methylbut-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56905-10-3
(E)-tert-butyl 4-chloro-2-methylbut-2-enoate

: 53689-87-5
t-Butyl-4-iod-2-methyl-trans-2-butenoat

Guidance literature:: With sodium iodide; In acetone;
DOI:10.1055/s-1976-24200

Reference yield:

: 56904-86-0
tert-butyl 2-(triphenylphosphoranylidene)propionate

: 53689-87-5
t-Butyl-4-iod-2-methyl-trans-2-butenoat

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂

2: NaI / acetone

With sodium iodide; In dichloromethane; acetone;
DOI:10.1055/s-1976-24200

Reference yield:

: 56905-19-2
tert-butyl 2-iodopropanoate

: 53689-87-5
t-Butyl-4-iod-2-methyl-trans-2-butenoat

Guidance literature:: Multi-step reaction with 4 steps

1: benzene

2: aq. KOH / benzene

3: CH₂Cl₂

4: NaI / acetone

With potassium hydroxide; sodium iodide; In dichloromethane; acetone; benzene;
DOI:10.1055/s-1976-24200